spectroscopy. The unknown ketone is from a homologous series of methyl ketones. CH3CO (CH2) nCH3 The first step in the lab is the preparation of the solvent used in the developing chamber for thin layer chromatography. The solvent used is a 3:1 mixture of toluene and petroleum. After the developing chamber is prepared‚ it is essential to begin preparation of the unknown DNPH derivative[6]. The preparation of the 1‚2 DNPH derivative of a ketone is in fact a small organic synthesis which produces a fraction
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Standardization of Solution and Titration Lab Report‚ Preparing a Dilute HCl Solution from a Concentrated One Titrating NAOH Solution with HCl Solution (of Known Concentration) Chemistry lab report(by abdazino abdalla) International College Objective preparing a dilute HCl solution from a concentrated one titrating NAOH solution with HCl solution (of known concentration) Procedure Section A: Preparation of 100.0cm3 0.480 mol/dm3 HCl solution a)Determine the volume of the concentrated acid
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ANALYTICAL AND ORGANIC CHEMISTRY LECTURER’S NAME : DR.RAPIDAH OTHMAN COD SUBJECT : NKB 10103 NAME : NUR NADIRAH BINTI BAHARUDEAN ID NUMBER : 55220114255 CHAPTER : ORGANIC CHEMISTRY CONTENTS 1‚4-BENZENEDICARBOXYLIC ACID Introduction The organic compound’s group that I’ve chosen in this assignment is 1‚4-benzenedicarboxylic acid. 1‚4-benzenedicarboxylic acid and also called as Terephthalic acid containing the carboxyl group and benzene group. Sometimes it simply referred to as a acid group
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The lab was to include a purpose‚ procedure‚ data/observations‚ all reactions and side reactions written out with qualitative data beneath each product and reactant except H20‚ and a summary. The purpose of this experiment is to observe the qualitative aspects of a series of reactions involving copper. Procedure 1.Measure about 1g of solid copper. 2.Place Cu in Erlenmeyer flask and place flask under fume hood. 3.Add dropwise 15M HNO3 until solid copper is completely reacted. 4.Place flask
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20 9. Classic chemistry experiments Unsaturation in fats and oils Topic Organic chemistry‚ saturated and unsaturated fats. Timing 45 min. Description The students titrate different oils and fats mixed with Volasil against bromine water. Apparatus and equipment (per group) w White tile w Conical flask w Dropper pipette. (Use the type of teat pipette usually fitted to Universal Indicator bottles‚ that do not allow squirting – eg Griffin.) w Burette (filled with bromine
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DENISTY LAB 2/25/13 Chemistry H. Mrs. Halme Objective: Your task is to determine the density of 3 known metals: Zinc‚ Copper‚ and Lead. They are each marked. You must then calculate the density of an unknown metal and determine its identity based on your data from your known samples. Reagents: None Equipment: Lead Copper Zinc Triple Beam Balance Graduated cylinder Unknown metal (Magnesium) Beaker Calculator Procedures Preparation: We observed the given equipment
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Organic Lab 1: Fractional Distillation Discussion: With the purpose of the experiment being to identify the 30 mL of unknown liquid‚ the theoretical basis of simple and fractional distillation must be deconstructed and applied to the data obtained describing the liquid in question. Simple distillation is a separation technique which can be used to separate and purify distillates from a liquid mixture which ideally contains one volatile and one non-volatile compound. If such ideal conditions are
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experiment is to practice common organic laboratory techniques inside the lab to get one oriented to the basic methods of procedure that can be used for later experiments. This experiment involves the separation of benzoic acid from a more crude form‚ consisting of benzoic acid‚ methyl orange‚ a common acid/base indicator‚ and cellulose‚ a natural polymer of glucose (Huston‚ and Liu 17-24). The technique that is used to perform this separation is called extraction. Extraction is a systematic process of
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Extraction of Caffeine from Tea Leaves using Dichloromethane (CH2Cl2) Abstract The extraction of caffeine (C8H10N402) was done in two parts. The first procedure used was solid-liquid extraction which was done by boiling the tea leaves in 100 ml. distilled water for 5-10 minutes. The filtrate was acquired and was extracted again by liquid-liquid extraction using dichloromethane (CH2Cl2). The combined DCM (CH2Cl2) was washed and dried to yield crude caffeine. The crude caffeine was purified
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Bioinformatics Leigh Ann Santana DNA Extraction Lab DNA extraction is an important process because the DNA first needs to be purified away from proteins and other cellular contaminants. Cell are needed‚ because that is where the DNA is located. Inside almost every cell in our bodies is a nucleus‚ and inside each nucleus is about two meters of DNA. The following steps are needed to purify DNA from a cheek swab. Collect cheek cells‚ Burst cells open to release DNA‚ separate DNA from proteins and debris‚ and
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