minimize this problem. The Objective of Research. The objective of this research is to synthesize and characterize eight ionic liquids using 1-methylimidazole as the starting material by using the alkylation and metathesis synthesis methods. H1-NMR and Ion Chromatography (IC) analysis will be used to verify the characteristic and presence of impurities to determine the purity of
Premium Solvent Water
Cheryl Baclit Chem 234 Experiment 4: Steam Distillation Introduction The purpose of this experiment is to extract Eugenol from Cloves using steam distillation as a purification technique and to transfer Eugenol from the aqueous phase to the MeCl2 phase. With steam distillation‚ the boiling point of a mixture of immiscible liquids is lower than the boiling points of the individual components. Water from the steam is one of the components of an immiscible liquid mixture. The vapor pressures of
Premium Water Distillation Laboratory glassware
utilizing this method of synthesis‚ the chemist has the knowledge to utilize certain chemicals to facilitate further reactions and derive pertinent data of said reactions by utilizing differing laboratory equipment‚ i.e.‚ nuclear magnetic resonance (NMR)‚ mass spectroscopy (MS)‚ infrared (IR)‚ and gas chromatography (GC) for analysis. These techniques allow the chemist to derive functional groups and isolate unknown compounds that can verify and identify unknown compounds often obtained through academic
Free Alcohol Ester Carboxylic acid
orange (the peel contains limonene‚ which is a terpene) and a dichloromethane solution of clove oil (which contains eugenol‚ an acetogenin). To isolate the eugenol‚ 20 mL of dichloromethane solution of clove oil was extracted twice; each time with a 15 mL portion of 3M NaOH. The aqueous extracts were then combined and acidified with approximately 17.6 mL of 6M aqueous HCl. Eugenol was isolated from the aqueous mixture by two extractions of 10 mL portions of dichloromethane. The dichloromethane extracts
Premium
cloves. Introduction By performing steam distillation we can isolate eugenol at lower temperature than its usual boiling point of 248 degree Celsius. Eugenol belongs to a category called essential oil. Many of these compounds are used as flavoring and perfumes and in the past were considered the essence of plant from which they were derived. Structure of eugenol (clove oil) and eugenol acetate: Reagents: Eugenol‚ CH2Cl2‚ Br2‚ FeCl3‚ Methanol Procedure: Co-distillation We first
Premium Distillation Essential oil Solvent
2.5. Characterization Methods 1H–NMR and 13C–NMR spectra of HPPP‚ BOMP and HVPA were taken in CDCl3 on Bruker DPX–300 MHz spectrometer using tetramethylsilane (TMS) as an internal standard. FT–IR spectra of the synthesized compounds‚ HPPP‚ BOMP‚ HVPA and photocrosslinked polymers were recorded on Perkin-Elmer system 2000 (4000–400 cm–1) spectrometer‚ using KBr pellets. Medium pressure mercury vapour lamp to the power output of 125W/cm2 was used for the photocrosslinking study. The viscosity of the
Premium Chemistry Spectroscopy Electromagnetic radiation
Lab Report Preparation Guidelines—IR Spectroscopy‚ General Unknowns‚ CH 315. Introduction/Purpose State in simple terms what the purpose was. Since one is issued a vial of an unknown substance‚ the “purpose” as such is not exactly in doubt. The object is simply to state that obvious purpose‚ as well as summarize (a comma-ed list here is fine) the various means‚ tests‚ so forth that are performed in the approximate order that they are performed. (approximately 10 points) Experimental
Premium Infrared
techniques were used to extract a crude‚ eugenol‚ and acetyleugenol product sample. These samples were submitted for GC analysis and the normalization area percents were calculated to confirm their purity; for the crude sample it was 93.95% eugenol and 6.05% acetyleugenol‚ for the eugenol sample it was 100% eugenol and 0% acetyleugenol‚ and for the acetyleugenol sample it was 24.84% eugenol and 75.16% acetyleugenol. The IR spectrum was also found for the eugenol and acetyleguenol products‚ which confirmed
Premium Distillation Chemistry Ethanol
fourth edition ORGANIC CHEMISTRY Francis A. Carey University of Virginia Burr Ridge‚ IL Dubuque‚ IA Madison‚ WI New York San Francisco St. Louis Bangkok Bogotá Caracas Lisbon London Madrid Mexico City Milan New Delhi Seoul Singapore Sydney Taipei Toronto | v v Boston | e-Text Main Menu | Textbook Table of Contents | Study Guide Table of Contents McGraw-Hill Higher Education A Division of The McGraw-Hill Companies ORGANIC CHEMISTRY‚ FOURTH EDITION
Premium Chemistry Organic chemistry Organic reaction
Compilation of “Dehydration of Methylcyclohexanol” Blog entries: A common Sophomore Organic Chemistry laboratory experiment that has great potential for further research is the acid catalyzed dehydration of simple alcohols. The classic dehydration of 2-methylcyclohexanol experiment that was introduced in Journal of Chemical Education in 1967 Taber(1967)JCE:44‚p620. The rather simple procedure of distilling an alcohol with an aqueous acid has spawned several investigations that have resulted
Premium Alcohol Chemistry