GRAVIMETRIC ANALYSIS Methods in GA Precipitation Method - involves isolation of an ion in solution by a precipitation reaction‚ filtering‚ washing the precipitate free of contaminants‚ conversion of the precipitate to a product of known composition‚ and finally weighing the precipitate and determining its mass by difference. From the mass and known composition of the precipitate‚ the amount of the original ion can be determined. Volatilization Method -the analyte or its decomposition products
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There are three main rock types present in Ireland: Igneous‚ sedimentary and metamorphic. Igneous rocks are rocks which have crystallized from molten rock. Sedimentary rocks are rocks which have formed due to the gradual accumulation of sediment. Metamorphic rocks are rocks which have once existed as igneous or sedimentary rocks but changed due to great heat or pressure. Over the course of my essay‚ I will account for five rocks found in Ireland and there probable rock forming conditions. Granite
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Preparation of Bromotriphenylmethane Abstract The structure of a major component of star anise oil was derived by analyzing its IR spectroscopy melting point of after oxidation and purification. From the evidence obtained‚ it was concluded that the exact structured should be p-methoxybenzoic acid. Introduction The purpose of this experiment is to determine the structure of the major component of star anise oil. It is already known that this component has a molecular formula C10H12O. This
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C│H│M│C│4│1 Letters 2013‚ Volume 1‚ Issue 1 A Perkin Reaction: Synthesis of (E)- and (Z)-Phenylcinnamic acids Thusanth Jogarajah‚ Dr. Lana Mikhaylichenko * Department of Physical and Environmental Sciences‚ University of Toronto Scarborough‚ 1265 Military Trial‚ Scarborough‚ ON‚ M1C 1A4 Received: February 6‚ 2013; E-mail Thusanth.Jogarajah@mail.utoronto.ca Abstract – Add text here Introduction: The name of this reaction is called the Perkin’s reaction. The reaction was
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poured onto about 10g of crushed ice in a beaker. 7.The product was isolated by vacuum filtration. The solid with a tiny amount of ice cold 50% methanol(mixture 1:1 methanol-water). 8.The crude product was recrystallized using methanol as the recrystallization solvent. 9.The yield and melting point were recorded. Results: Weight of filter paper = Weight of filter paper + crystals = Weight of crystals = 2.1594g Melting point of crystals = 79°C Density of methyl benzoate = 1.094g/mL Mass of methyl
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INTRODUCTION Thermotherapy‚ Mechanotherapy and Hydrotherapy are used as treatments to help relieve pain and help relax clients. Thermotherapy is formed by using heat in a treatment for the intention to change the core temperature of the soft tissue with the purpose of improving symptoms of certain conditions. Mechanotherapy is a treatment using hand and instrument methods used for smoothing‚ pressure and stretching to improve cell metabolism‚ hep blood circulation and pain. Hydrotherapy is a treatment
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PRODUCTION OF CITRIC ACID Introduction: Citric acid is a White solid‚C3H4OH(COOH)3‚soluble in water and slightly soluble in organic solvents‚ which melts at 153 oC. Aqueous solutions of citric acid are slightly more acidic than solutions of acetic acid. Traces of citric acid are found in numerous plants and animals‚ because it is a nearly universal intermediate product of metabolism. Large amount of the acid are found in the juice of citrus fruits‚ from which it is precipitated by the
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English Proficiency This test is designed to assess the test takers’ general proficiency in the use of English language as a means of self-expression in real life situations and specifically to test the test takers’ knowledge of basic grammar‚ their vocabulary‚ their ability to read fast and comprehend‚ and also their ability to apply the elements of effective writing. 1. Grammar 1. Agreement‚ Time and Tense‚ Parallel construction‚ Relative pronouns 2. Determiners‚ Prepositions‚ Modals
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curve was linear over the range 0.1-5.0μg/ml. The method was also suitable for the assay of paracetamol-codeine combination drug as well as estimation of the amount of constituents in urine when the wavelength of UV detection was 245 nm with acetanilide as the internal standard. Keywords: Chromatography‚ isocratic‚ internal standard‚ in vivo and in vitro INTRODUCTION Paracetamol (N-(4-hydroxyphenyl) acetamide) tablets are listed among the essential drugs selected for the health care delivery
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tetraphenylcyclopentadienone using a reaction of dibenzyl ketone (1‚3-diphenyl-2-propanone) with benzil in the presence of base. The reaction then proceeded with an aldol condensation reaction.5 This product was obtained using extraction (reflux)‚ recrystallization and vacuum filtration to separate the product from the waste. Experiment Scheme: Figure 1: Experiment Reaction5 Figure 2: Step wise reaction mechanism including aldol condensation reaction5 Procedure: About 1.55-g of benzil‚ 1.51-g of
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