Organic Chemistry II Laboratory (ABCT357) Although studying fundamental theories of chemistry in the class is important to understand the concept of chemistry‚ carrying out experiments to corroborate the theories is also important. It is very important for students to get used to experiments in order to speed up their experiments. Expt.1. Acetylation of α-D-glucopyranose Add slowly 2.5 g (0.014 mol) of powdered D-glucose in small portions (roughly in 7-10 portions and 5 min for each addition)
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Chem 105 Guide to the Formal Laboratory Report The purpose of a formal report is to communicate effectively to another person the goal‚ procedure‚ data analysis method‚ and results of your laboratory work. The report is divided into several well-defined sections. Each section must be present in a complete report. To earn an outcome point for the laboratory report‚ a student must submit a formal lab report that earns a score of at least 90/100. Each error (factual‚ grammatical‚ typographical
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Experiment 22: Synthesis of Aspirin and Oil of Wintergreen Performed 01/31/2013 Received 02/07/2013 Organic molecules have a wide range of applications occur both intracellular as well as in many different industries. The reactions use the reactivity of functional groups attached to organic molecules‚ as well as general chemistry concepts such as Le Chatelier’s Principle (). The synthesis of Aspirin (its chemical name being acetylsalicylic acid) and of oil of wintergreen (with its chemical
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Tris(acetylacetonato)manganese Dissolve 0.26 g manganese(II) chloride tetrahydrate and 0.68 g of sodium acetate in 10 mL of distilled water. Add 1 g acetylacetone and swirl the mixture. With magnetic stirring‚ add dropwise a solution of 0.052 g potassium permanganate in 2.5 mL of distilled water over a period of 10-15 minutes. Stir for 10 minutes‚ then add dropwise a solution of 0.63 g sodium acetate in 2.5 mL distilled water. Heat the resulting mixture on a hot plate to between 60 and 70oC for
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Objective: The target of this study was to evaluate the anthelmintic and antimicrobial activity of synthesissed quinoxaline-2‚3-Dione. Methods: The anthelmintic activity of selected newly synthesized 2‚ 3-dioxo-1‚ 2‚ 3‚ 4-tetrahydro quinoxaline-6-sulfonyl benzimidazole (s) were performed on adult earthworm (Pheretima Posthuma). The observation was made for the time taken to paralysis and/or death of individual worms up to four hours of the test period. Paralysis was said to occur when the worms
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Wittig Reaction and Photoisomerization Abstract: For this laboratory experiment stilbene was produced through a Wittig reaction with benzyltriphenyl phosphonium and benzaldehyde producing a form of stilbene (Figure 1). This reaction favored a crude Z-Stilbene crystal product over its E counterpart. When Z-Stilbene underwent photoisomerization with iodine for 1 hour it reconfigured almost exclusively into its more stable counterpart E-Stilbene. The reaction produced very low yield of 6.3% due
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Carbonate Rocks and Dunham’s Classification Palkowski‚ Daniel N. 245-002 General Geology Dr. Wayne Schlipp 9 December 2007 Abstract The following contains a compendium of research on carbonate rocks. Displayed are a basic description of carbonate rocks‚ depositional environments‚ mineralogy‚ ancient and modern reefs‚ diagenesis‚ facies analysis‚ and classification. Most carbonate rock classification schemes take into account characteristics that may require intensive microscopic
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EXP-10 CHEM 233L SYNTHESIS OF p-BROMOANILINE Introduction: In this experiment‚ p-bromoaniline was synthesized in three steps starting from aniline. Since the amino group of aniline is a strong activator of aromatic ring‚ direct bromination is impractical (equation 1). In order to make a desired product‚ amino group needed to be protected as the acetamide which also maintained ortho and para position but slowed down the rate of reaction (equation 2). Slow reaction rate would increase
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Dating Dating techniques are procedures used by scientists to determine the age of a specimen. 2 types of Dating: *Relative Dating *Absolute Dating Relative Dating -methods tell only if one sample is older or younger than another sample. -They do not provide an age in years. Stratigraphy -Main Relative Dating Method -is the study of layers of rocks or the objects embedded within those layers. -based on the assumption that deeper layers were deposited earlier‚ and thus are older than
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Lady Jewellyn G.Diola*‚ Jennika Joy L. Casin‚ Andrian R. De Leon‚ Jan Rotsen Kyle A. Delos Santos Department of Chemistry‚ College of Science *Lady Jewellyn G. Diola; ladyjewellyndiola@yahoo.com Abstract Synthesis of 3‚4-dihydro-3-(p-methylphenyl)-1‚2-(2h)-benzoxazine involves the nucleophillic addition of the 1 °amine group upon the carbonyly group of the salicylaldehyde‚ the reduction of imine to amine and the addition of paraformaldehyde to proceed ring closure. The
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