Theo Victor Cavite Chem 28.1 Melanie Bucsit-Carpio September 14‚ 2012 Spectrophotometric Determination of Iron in Aqueous Solutions as a Complex of 1‚10-Phenanthroline Introduction From the previous classical method of concentration determination of an unknown sample‚ this experiment now deals with the instrumental one. Unknown concentrations of iron in solutions were determined by measuring their corresponding absorbances through spectrophotometry. A spectrophotometer measures the amount
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Experiment A Spectroscopic determination of Iron with Phenanthroline Unknown # 2 Mass of Mohr’s Salt: 0.2040 1. 5mL of 6M acetic acid was measured and transferred into a 100mL volumetric flask with a pipette and diluted to the mark. Concentration = [0.2040(±0.0001)g/100(±0.08)mL]*[(1mol/392.16g)/(1L/1000mL)] = 0.005202(±0.09382%) = 0.005202(±0.000005)mol/L 2. 10mL of the above stock solution was transferred to a 250 mL volumetric flask and diluted to the mark. Concentration
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Spectrophotometric Methods: The Determination of Iron The goal of this laboratory experiment was the quantitative spectrophotometric determination of Fe (II) by using a calibration plot‚ which obeyed the Beer-Lambert Law. In order to determine the Fe (II) concentration‚ a series of solutions of known concentrations were made. The solutions were analyzed by the Ocean Optics spectrophotometer in order to determine their absorbance. The concentration of the unknown Fe (II) was determined by the “eye-ball”
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ESTIMATION OF IRON IN IRON ORE-SPECTROPHOTOMETRIC METHOD By: Taylor Villari Experiment conducted on 7/22/13 Components of each test tube examined in the spectrophotometer Trial | Volume of Iron solution (mL) | Micrograms of Iron | Volume of 10% sodium acetate | Volume of 0.1% o-phenanthroline | Volume of water (mL) | 1(blank) | 0.0 | 0.0 | 1.0 mL | 1.0 mL | 8.0 mL | 2 | 1.0 mL | 10 | 1.0 mL | 1.0 mL | 7.0 mL | 3 | 3.0 mL | 30 | 1.0 mL | 1.0 mL | 5.0 mL | 4 | 5.0 mL | 50 | 1.0 mL
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Lab 2: Spectrophotometric Determination of Iron In Vitamin Tablets Objectives: - To determine the amount of iron in a generic vitamin tablet on a per tablet (in grams) basis. - To prepare standards using a pre-made iron solution to help determine the iron content in our generic vitamin tablets - Determine absorbances of our vitamin tablets and standards using the spectrophotometer Method: 1. Mass three vitamin tablets that contain iron 2. Place each vitamin in a 125-mL Erlenmeyer flask
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Spectrophotometric Determination of an Equilibrium Constant Introduction: In this experiment‚ you will study the reaction between aqueous iron (III) nitrate‚ Fe(NO3)3‚ and potassium thiocyanate‚ KSCN. They react to produce the blood-red complex [Fe(SCN)]2+. Fe3+ + SCN- ( [Fe(SCN)]2+ The equilibrium constant expression may be expressed as: K = [pic] You will prepare a series of standard solutions that contain known concentrations of [Fe(SCN)]2+ and will determine
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The Spectrophotometric Determination of an Equilibrium Constant. Abstract: The report presents determination of equilibrium constant for the formation of a complex ion FeSCN2+. This was accomplished using a colorimeter to measure absorbance of some known concentration solutions in order to generate the calibration curve. The equation of the graph was used to compute the equilibrium concentrations of the reactants and products‚ needed to calculate the equilibrium constant for
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Spectrophotometric Determination of Equilibrium Formal Report Matt DeLuca The Department of Chemistry‚ SUNY College at Brockport Brockport‚ NY 14420 CHM 206.04 Abstract: The main objective of this experiment was incorporating the use of spectrophotometry in an attempt to study the position of equilibrium. Furthermore‚ after the completion of this experiment‚ the formation of the equilibrium constant of the iron thiocyanate complex
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Title: Determination of Iron in Natural water by Spectrophotometry. Aim: To determine the iron in natural water by spectrophotometry. Abstract: The iron in natural water was determined by utilizing spectrophotometric analysis. That was done by measuring the absorbance of five Fe(oPH)2+3 standards at 510 nm. From that information‚ a calibration curve was plotted and used to find the amount of Fe2+ that was in two unknown water samples based on the absorbance readings obtained with them at 510nm. The
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Spectrophotometric Determination of the Equilibrium Constant of a Reaction DEPARTMENT OF MATERIALS‚ METALLURGICAL AND MINING ENGINEERING‚ COLLEGE OF ENGINEERING July 26‚ 2012 ------------------------------------------------- ABSTRACT ------------------------------------------------- Before proceeding to test the next solution‚ we must first clean the cuvette‚ using similar steps earlier. First‚ we rinse with water‚ then with the solution‚ and then we fill it up and test
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