SYNTHESIS OF THE PHARMACEUTICAL ASPIRIN (ACETYLSALICYLIC ACID) AIM: The aim for this experiment was to synthesise a small amount of aspirin with salicylic acid as the starting product and sulphuric acid as the catalyst. The product obtained from this reaction will be impure and will need to be purified. This will be done by recrystallization. We will then record the products’ melting point and calculate the yield in order to determine the degree of purity of the aspirin sample. Diagrammatic scheme
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DNA synthesis inhibitors Nucleic acid inhibitors are chemicals which inhibit the production of nucleic acids including both DNA and RNA. DNA and RNA inhibitors inhibit enzyme action in DNA replication in the same way as the topoisomerase inhibitors we discussed earlier. Topoisomerase inhibitors (1) (10) are chemicals which interfere with the enzymes that allow DNA strands to separate and to re-join‚ a process that is required for the division of bacteria and without which DNA cannot effectively
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a Grignard compound with the reagents bromobenzene and magnesium metal. The bromobenzene was first transformed into the Grignard compound and was then reacted with the benzophenone to make the final product. The mixture was then mixed with sulfuric acid and the organic layer was extracted via a separatory funnel. The mixture was then recrystallized from methanol and was allowed to dry and the percent yield‚ melting point‚ and the IR was obtained. The mass of the product obtained was 5.45 grams and
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Synthesis of Banana Flavor CHEMISTRY 200L EXPT 02 PAGE 01 - 11 Gerome B. Vallejos*‚ Ellis Mika C. Trino‚ Jahn Camille B. Valdez‚ Ariza Yamashita Department of Biological Sciences‚ College of Science Group 11 Corresponding author: gerome_911@yahoo.com Abstract The purpose of this experiment was to synthesize isopentyl acetate via Fischer esterification reaction between acetic anhydride and isoamyl alcohol‚ using concentrated sulfuric acid as a catalyst. This reaction is characterized by the combining
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------------------------------------------------- Hydrochloric acid From Wikipedia‚ the free encyclopedia (Redirected from Muriatic acid) Not to be confused with hydrogen chloride. Hydrochloric acid | | | | Other names[hide] * Muriatic acid[1] * Spirits of salt[2] | Identifiers | CAS number | 7647-01-0 | ChemSpider | 10633809 | UNII | QTT17582CB | EC number | 231-595-7 | ChEMBL | CHEMBL1231821 | ATC code | A09AB03‚B05XA13 | Properties | Appearance | Colourless
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References: (1) Alkyl halides. Retrieved from http://hyperphysics.phy-astr.gsu.edu/hbase/organic/alkhal.html (2) Arnold‚ H.R. & Lessig‚ E.T. Synthesis of alkyl halides. United States Patent Office: 1937. (3) Bauld‚ N.L. Alkyl halides. 2001 Retrieved from http://research.cm.utexas.edu/nbauld/teach/halides.html#mechanism (4) McGraw-Hill Companies. Preparations of alkyl halides. Retrieved from http://www
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Lactic Acid Bacteria Amanda Perry Many persons are oblivious to the fact that when they consume certain delicious food products like yogurt‚ buttermilk or cheese‚ they are actually eating live bacterial biomass which has acidified the milk content and contains a mixture of bacterial slime layers. Perhaps it is a blessing that most people are unaware because when most hear the word ‘bacteria‚’ their first thought is of a microscopic unicellular organism that causes various types of diseases especially
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Synthesis of Methyl Salicylate from Aspirin Esters are a class of organic compounds. An ester compromises an organic or inorganic acid in which one or more hydroxy (OH) groups have been replaced by and alkoxy (O-alkyl) group. For example‚ the simplest ester‚ methyl formate (CHOOCH3)‚ is made up of formic acid (CHO-OH) in which the hydroxyl group has been replaced by a methoxy group (-OCH3). Similarly‚ ethyl acetate (CH3CO-OCH2CH3) is made up of acetic acid (CH3CO-OH) in which the hydroxy group
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Isopentyl Acetate Synthesis Results: Crude % Yield Calculation Reaction: H2SO4 C2H4O2(aq) + C5H12O(aq) ----> C7H14O2(aq) + H2O(l) (1 mole of acetic acid reacts with 1 mole of isopentyl alcohol to make 1 mole of isopentyl acetate and 1 mold of water) Volume of isopentyl alcohol (d=0.809g/mL; MW=88.15g/mol): 2.5mL Moles of isopentyl alcohol: (2.5mL)(0.809g/1mL)(1mol/88.15g) = 0.02294mol Volume of glacial acetic acid (d=1.06g/mL; MW=60g/mol): 3.5mL Moles of glacial
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Activity 1.7.2 Synthesis of Esters Purpose- the Purpose of this lab is to synthesize Esters by combining Carboxylic Acid and Alcohols. In this lab we will synthesize and then detect the odour of Esters formed. Materials- Materials that will be used in this lab are as follows:- Ethanol 7. Acetic Acid Eye Protection 11. Test tube rack Procedure- Prepare a hot-water by half filling a 500-mL beaker with water and heating it carefully on a hot plate until it comes to a gentle
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