First‚ the synthesis of the coordination compound‚ KaFeb(ox)cdH2O‚ needed to be carried out. This was achieved by weighing out 8.29 grams of K2C2O4 with a Dial-a-gram balance. Once measured‚ the 8.29 grams K2C2O4 were placed in a 125 mL Erlenmeyer flask. 25 mL of deionized water were then added to the 125 mL flask and stirred with the K2C2O4 until complete dissolution was achieved. Next‚ 4.11 grams of FeCl3 were weighed out using the balance previously mentioned. Once the 4.11 grams were measured
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Abstract Oxidation was found for primary alcohol. When 6 drops of potassium dichromate and 1 drop of concentrated sulfuric acid were added to 1-pentanol‚ the color of 1-pentaol turned into dark green. In second experiment‚ precipitation was found when 6 drops of 2‚4-dinitrophenylhydrazine were added to both 5 drops of benzaldehyde and 5 drops of acetophenone. Based on these data‚ it is possible to find alcohol by oxidation and aldehyde by observing precipitation Introduction This experiments
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mL of unknown #12. The flask was then covered and had a hole poked through the foil. Next‚ it was placed into boiling water. After the liquid was fully evaporated it was taken out‚ wiped dry and‚ allowed to cool. Then the mass was measured. Then the lab station was cleaned and the waste properly disposed of.
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Acetyl chloride‚ CH3COCl‚ also known as ethanoyl chloride or acyl chloride‚ is an acid chloride derived from acetic acid. It belongs to the class of organic compounds called acyl halides. It is a colorless liquid. Acetyl chloride does not exist in nature‚ because contact with water would hydrolyze it into acetic acid and hydrogen chloride. In fact‚ if handled in open air it gives off white smoke owing to the hydrolysis from the moisture in the air. The "smoke" is actually small droplets of hydrochloric
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Experiment 1 Synthesis of Acetaminophen Clifford Tse 20529845 Partner – Raminder Dhanoa TA – Xiao Qi CHEM 123L - 012 February 6‚ 2014 Introduction Acetaminophen‚ also commonly known as Tylenol‚ is an over-the-counter medicine used to relieve pain and reduce fevers. Within this experiment‚ Acetaminophen will be formed through the reaction between p-aminophenol and acetic anhydride. This reaction will incur Acetaminophen as a crude solid being impure‚ which will be purified further through
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Abstract: The purpose of this lab is to synthesise acetylsalicylic acid (aspirin) by creating a reaction between acetic anhydride and salicylic acid. This was be accomplished through the use of recrystallization. Acetic anhydride and salicylic acid are mixed together‚ and then acidified by the addition of a few drops of concentrated sulfuric acid‚ which catalyzed the reaction. The percent yield is calculated to determine the effectiveness of the reaction in preparing the desired product (aspirin)
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In our ecocolumn many changes occurred over the several week course we were observing and collecting data on the three chambers. Aquatic and Decomposition quickly turned septic while terrestrial experienced plant growth. Overall the health of the ecosystem was very poor due to the severe changes in the aquatic chamber. Terrestrial In the Terrestrial camber of our ecocolumn‚ several changes happened over time. The clover seeds planted at the beginning had a rapid growth rate. At one point our chamber
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product had no color changes and remained orange when mixed with the iron (III) chloride solution‚ which means that there were no phenol groups in both the crude aspirin product and the purified aspirin product. The lack of reaction with the iron (III) chloride revealed that both the crude aspirin product and the purified aspirin product were pure aspirin. The salicylic acid turned
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Purpose Acetophenetidin can be formed through two methods‚ Williamson ether synthesis and amide synthesis. By working in groups of two we were able to complete both methods of synthesis routes. The end result should be the synthesis of a similar product‚ by verification between the two individuals. Reaction Experiment and Observations Amide Synthesis of Acetophenetidin The Synthesis reaction began by removing the colored impurities from the p-phenetidine‚ accomplished by mixing
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Synthesis of Aspirin (Acetylsalicylic Acid) Abstract: This experiment is about the synthesis of aspirin under laboratory conditions. Aspirin is prepared by reacting salicylic acid and acetic anhydride; in the presence of sulfuric acid. After fully dissolving the salicylic acid with acetic anhydride‚ the solution is cooled and cold water is then added. Once the crystals form they are then filtered and left to dry out. There mass is measured and recorded then the yield is calculated. Introduction:
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