PurposeIn this experiment‚ sodium hypochlorite (NaOCl) in acetic acid mixture was used to oxidize emdo-borneol (an alcohol) to camphor (a ketone). The product would then be purified by sublimation and then be analyzed by Infrared spectroscopy and melting point test. Procedure and ObservationsPlease refer to the lab manual and the carbon copy attached. Data and CalculationsWeight of endo-borneol = 0.2013gNo of moles of endo-borneol = 0.2013g/154.25g mol-1 = 1. 305mmolSince one mole of endo-borneol
Premium Chemistry Chlorine Sodium hydroxide
A- HPTLC Flavonoid profile of methanol extract M. concanensis leaves B- HPTLC Flavonoid profile of methanol extract M. concanensis flowers C- HPTLC Flavonoid profile of methanol extract M. concanensis seeds 4.2.3.1 C) HPTLC Phenol profile of M. concanensis Nimmo. HPTLC finger printing of M. concanensis was done by using selected solvent system Chloroform: Ethyl acetate: Formic acid (50%:40%:10%v/v) for leaf‚ flower and seed extracts‚ visualized under UV 254 and 366 nm showed more
Premium Carboxylic acid Alcohol Acetic acid
TITLE: Determination of Riboflavin by using UV-Vis spectrophotometry. ABSTRACT: The amount of Riboflavin in various brand of children multivitamins was determine by using UV-Vis spectroscopy instrument‚ the series of standard of riboflavin was prepared in order to determine the amount of the riboflavin in the sample of children multivitamins. The maximum amount of riboflavin was found in the Champs multivitamin that contains 0.1155 mg followed by Chewies 0.1131 mg and Scott’s 0.0672 mg. OBJECTIVES:
Premium Acetic acid Vitamin Vitamins
a one-pot synthesis. The process of synthesis involved the use of butyl amine‚ carbon(IV) sulfide and sodium hydroxide at a temperature < 0oC. Crystals were obtained and the compound was characterized with elemental analysis‚ Fourier infra-red spectroscopy (FT-IR)‚ Ultra-violet visible (UV-VIS)
Premium Chemistry Acetic acid Oxygen
as well as ultraviolet and infrared regions. Photochemistry‚ a sub-discipline of chemistry‚ is the study of the interactions between atoms‚ small molecules‚ and light (or electromagnetic radiation).[1] The pillars of photochemistry are UV/VIS spectroscopy‚ photochemical reactions in organic chemistry and photosynthesis in biochemistry. |Contents | |[hide] | |1 Scientific background | |2 Spectral
Free Photosynthesis
be the product of the reduction reaction because of steric hindrance. For the oxidation step‚ a reflux will be done and then a microscale reflux for the reduction step. The products will be confirmed using Infrared spectroscopy‚ the chromic acid test‚ 2‚4-DNP test and 13C NMR spectroscopy. The results of this experiment show that camphor was produced during oxidation (0.6576 g). The IR spectrum shows a strong peak at 1740 cm-1 representing a carbonyl compound‚ which was concluded to be a ketone by
Premium Alcohol
treat this increased volume‚ and thus the final amount of product was larger than intended and was not as effectively dried with anhydrous sodium sulfate as was desirable. Because of this‚ the TA advised adding extra filter papers‚ which led to the absorption of the exo-norborneol into them. The exo-norbornenol condensed as liquid droplets on the petri
Premium Chemistry Solvent Diethyl ether
Chapter II Light and Matter The Inner Workings of the Cosmos 2.4 The Distribution of Radiation All microscopic objects – fires‚ cubes‚ people‚ and stars – emit radiation at all times. They radiate because the microscopic charged particles in them are in constant random motion‚ and whenever charges change their state of motion‚ electromagnetic radiation is emitted. The temperature of an object is a direct measure of the amount of microscopic motion within it. The hotter the object
Free Electromagnetic radiation Light Electron
Polymer Chemistry Course‚ KTE 080‚ 2014 Patric Jannasch ———————————————————————————————— Laboratory procedures in polymer chemistry Polymer & Materials Chemistry 1. Free Radical Bulk Polymerization of Styrene This protocol describes the bulk polymerization of styrene at 60 oC using 2‚2´azobisisobutyronitril (AIBN) as an initiator. The monomer styrene first has to be purified before it can be used. The purification is performed in order to remove inhibitors and impurities‚ which can
Premium Polymer Monomer
carotenoid family play integral roles in plants. They use the absorption of light to aid in photosynthesis‚ and protect chlorophyll from damage. In humans‚ Lycopene acts as an antioxidant. Lycopene is found in various fruits and vegetables. The purpose of this experiment is the isolation of Lycopene from tomato paste. This is done using liquid/solid extraction and chromatography. Once the Lycopene is isolated‚ IR spectroscopy will determine its percentage actually obtained by chromatography
Premium Lycopene Laboratory glassware Photosynthesis