CHM152LL LAB MANUAL COMPLEXOMETRIC DETERMINATION OF WATER HARDNESS Complexometric Determination of Water Hardness Introduction Complex ions When a neutral molecule or anion (a Lewis base) donates electron pairs and attaches itself to a metal ion center (a Lewis acid)‚ the resulting cluster‚ or complex‚ of atoms becomes a single complex ion. When such complexes form‚ the electron donating groups (called ligands) form coordinate covalent bonds through empty orbitals on the metal ion. An example
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Complexometric Determination of Water Hardness 9/12/2013 Abstract: Two sets of acid-base neutralization titrations were conducted for experimental analysis. The first set of titrations was to standardize a solution manufactured in the lab. An approximate solution of Na2EDTA of 0.004 M was titrated against a known solution of 1.000 g CaCO3/L to deter mine to exact molarity of the Na2EDTA. Ca2+ + Na2EDTA → CaEDTA + 2Na+ The second set of titrations was to use the now standardized Na2EDTA
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central metal ion. In this experiment‚ the affinity of EDTA for metal ions will be applied to tap water that has a particularly high mineral content. Through chelometric (complexometric) titration‚ EDTA can be used to gauge the concentration of metal wastes found within hard water. Eriochrome Black T will be used to indicate when the EDTA has fully absorbed the metal impurities found in the hard water. H2In- + M2+ (aq) ↔ MIn- (aq) + 2H+ (aq) H2In- is the Eriochrome Black T in its normal form
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Experiment 2 Title: Determination of Quinine in Tonic Water Objective: To Determine the Concentration of Quinine Hydrochloride in Sample (Schweppers) given‚ by plotting a Calibration Curve of Fluorescent Intensity against Concentration of Quinine Hydrochloride in ppm‚ after Fluorescence Intensity of a series of Standard Solution prepared and the Sample solution by Fluorescence Spectrometer. Data: Brand name of tonic water sample: Schweppes Dilution factor = 1000 Concentration of
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precipitate with alcoholic silver nitrate (Q.2) Dry ether The reaction RX + 2Na + RX _______________? R-R + 2NaXis called. ( 1 mark ) (a) Sandmeyer’ reaction (b) Fittig reaction (c) Wurtz reaction (d) Williamson’s synthesis (Q.3) Substitution of chlorine takes place readily at higher temperature in : ( 1 mark ) (a) CH3CH=CH2 (b) H2C=CH2 (c) HC C (d) None of the above (Q.4) (CH3)3CMgBr on reaction with D2O gives: ( 1 mark ) (a) (CH3)3CD (b) (CH3)3COD (c) (CD3)3CD (d) (CD3)3OD (Q.5) The silver
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Complexometric Determination of Water Hardness Kayla Partridge Britni Gonzales 09/15/2014 Abstract Determining the water hardness of unknown sample #55 was determined by complexometric titration. With the use of disodium salt EDTA as the solution to chelate the metal impurities and the Eriochrome Black T indicator as the solution used to help visualize when the impurities were completely chelated‚ along with a few other solutions to help the reaction. Unknown water sample #55 experimental
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results indicate that the unk B tap water can be considered as hard water. INTRODUCTION Hard water is due to metal ions (minerals) that are dissolved in the ground water. These minerals include Ca 2+‚ Mg2+‚ Fe3+‚ SO42-‚ HCO3-. When this water evaporates or boils‚ the difficult to dissolve metal salts remain as a scaly residue. Hard water inhibits the effectiveness of soap and detergents. Calcium ions typically make the most significant contribution to water hardness. This is why hardness is
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In order to prepare the iodine solution titrant‚ exactly 50 mL of 0.01 M KIO3‚ exactly 20 mL of 10% KI solution‚ and exactly 25 mL of 0.3 M H2SO4 was transferred into a 100 mL volumetric flask using a volumetric pipette. The volumetric flask was then filled to the mark with distilled water. The flask was covered with Parafilm and inverted to mix. The next part of the experiment was to determine the Vitamin C in a solution of known concentration. Observations of the Vitamin C sample and the amount
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1 October 2010 Salt Water Pool Systems vs. Liquid Chlorine Pool Systems I currently utilize a salt water pool system called an Aqua Rite System. If you’re in the market for a pool‚ it can be a bit overwhelming to choose a type of system that is right for you. The salt water pool vs. chlorine pool battle has been raging over the last decade‚ and today‚ many home owners are building these systems right from the start or converting their old chlorine pools into a salt pool. But what is the real
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Many advanced high school and college chemistry students perform an experiment known as the "iodine-clock" reaction‚ in which hydrogen peroxide reacts with iodide to form iodine‚ and the iodine subsequently reacts with thiosulfate ion until the thiosulfate has been consumed. At that point‚ the reaction solutions turn blue in the presence of starch. The experiment helps students understand the fundamentals of chemical kinetics --- the speeds at which reactions take place. 1. Activation Energy
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