the hydrate copper (II) sulfate and the anhydride we were able to determine the mass of water in the hydrate. This information was then used to determine the empirical formula of the hydrate‚ defined as a compound formed by the addition of water to another molecule. In the first trial‚ the mass of water in the hydrate was determined to be 0.41 g‚ while in the second trial the mass of water was 0.52 g. Moles of water associated with a single mole of anhydride were then calculated for both trials‚ giving
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other to react twice with a Grignard followed by removal of the protecting group by acid hydrolysis to give final product (C2). Method: Ethyl acetoacetate (30.03g)‚ ethylene glycol (15.01g) and toluene-p-sulphonic acid (0.13g) were added to a 250 cm3 round bottomed flask‚ containing a stirrer bar and toluene (100 cm3)‚ fitted with a condenser and dean-stark head. Solution was heated strongly under reflux using a heater stirrer block for approximately one hour. During heating 4.5 cm3 of water was collected
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acetaminophen. p-aminophenol and acetic anhydride were used to create acetaminophen and acetic acid. The acetic acid mixed with acetaminophen created an impure sample‚ which was purified through the addition of a water/methanol solution. The percent recovery of acetaminophen from the impure sample to the pure sample was 76%. The melting point of the pure sample was 167C - 169C. Introduction: Formulation of acetaminophen involves treating an amine with an acid anhydride to give rise to an amide. In this
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Department of Occupational Therapy‚ College of Rehabilitation Sciences University of Santo Tomas‚ Espaňa Street‚ Manila 1008 Date Submitted: February 2‚ 2011 Abstract: Organic compounds hexane‚ heptane‚ cyclohexane‚ cyclohexene‚ benzene‚ and toluene were subjected to different physical and chemical tests todifferentiate their intrinsic physical properties and chemical properties in terms ofstructure and behaviour. Nitration test (test for the presence of aromatic ring)‚ Bromine test (test for
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Preparation of Acetylsalicylic Acid Abstract Acetylsalicylic acid was prepared using salicylic acid and acetic anhydride. As a result‚ a white‚ powdery substance was formed (0.1931g‚ percent yield 91.30%) and was defined by melting point (124.5 – 134.5°C) and observation of color change with ferric chloride. Introduction Acetylsalicylic acid (aspirin) is one of the most popular analgesic drugs on the market today. It also acts as an antipyretic and anti-inflammatory drug. Salicylic acid itself
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prepare the water bath‚ ice bath and a fluted filter paper while others were tasked to weigh the filter papers in advance so that the experiment will flow smoothly. The formation of crude acetanilide was due to the acetylation of aniline and acetic anhydride. The recrystallizing solvent dissolved the acetic acetanilide and was heated in a water bath. Crystals started to form after cooling the solutions in an ice bath. Pure acetanilide was the product after the second crystrallization which was obtained
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These modifications are grafting‚ alkylation-especially esterification including acetylation. The purpose of the project is to prepare acetylated starches/starch esters of different Degree of Substitution using different concentrations of acetic anhydride for modifying the native starch. The testing of samples is done by testing various properties of the obtained samples such as Degree of Substitution‚ Solubility‚ Swelling Power‚ Light Transmittance and Water Binding Capacity. INDEX
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β-D-Glucose Pentaacetate from its Original D-Glucose and it comparison with literature though Melting point‚ TLC‚ IR‚ 1H and 13C NMR Abstract: The synthesis of the product: β-D-glucose pentaacetate is done though the acetylation using acetic anhydride with D-glucose with the help of sodium acetate. The recrystallization of the product is done though a polar solvent like water. The Result of this experiment has a percentage yield of 61% and analytical methods that are to detect the products are
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uses‚ which include; reducing fevers‚ reducing headache pain‚ relieve swelling and joint pain often associated with arthritis‚ enhances the elimination of uric acid. Acetylsalicylic acid‚ aspirin‚ is prepared by reacting salicylic acid with acetic anhydride:  Figure 1. Chemical Equation for Aspirin Synthesis (Aspirin) Tylenol‚ acetaminophen‚ is also used both as a fever reducer and pain reliever. Acetaminophen is prepared by reacting ammonia with acetic acid:  Figure 2. Chemical
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contrasting the psychoanalytic theories of Sigmund Freud‚ Carl Gustav Jung‚ and Alfred Alder‚ I felt like Sigmund Freud had the most‚ wide range of theories and the broader range of thoughts throughout his readings. One thing that Alder touched on that puzzled me is the fact that we all some kind of way are coming into our personality as a child while suckling on our moms breast. Another thing that puzzled me about Alder is that our personality comes from a form of sexuality‚ like the comment he made about
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