reactivity of hydrocarbons to functional group tests; Bayer’s test‚ Bromine test light‚ Bromine test dark‚ and Tollen’s test. In Bayer’s test‚ only Acetylene‚ Eugenol and Unknown hydrocarbon 2 reacted positively and the rest retain the purplish color of KMnO4. On the other hand‚ the five compounds in Bromine test with light reacted positively. In Bromine test dark‚ Hexane and Unknown hydrocarbon 1 did not react because light (UV) is absent. Lastly‚ in Tollen’s reagent‚ only Acetylene reacted positively
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Materials:1). 0.02 mol dm-3 Potassium Manganate2). 0.2 mol dm-3 Glucose3). 2 mol dm-3 Sulphuric Acid4). 50 cm3 Burette5). 250 cm3 Beaker6). Measuring Cylinder7). Thermometer (-10 to 110 oC)Hypothesis:By adding glucose to a solution of KMnO4 and H2SO4‚ the solution will turn colourless and it will take a specific time for the reaction to complete. By increasing the temperature‚ the time it takes (the rate) for the solution to completely change to colourless will be increased. Thus it can be said‚
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solid crystals 95% ethanol Clear colorless liquid Acetyl chloride Clear colorless liquid with gas escaping from container FeCl3 Clear colorless liquid Commercial aspirin Fine powdery white solid crystals I2/KI Deep black liquid KMnO4 Brownish liquid Phosphoric acid Clear colorless liquid Table 2. Preparation of Aspirin. Description Salicylic acid + Acetyl chloride Cloudy white liquid with undissolved white powder Mixture at room temp White cloudy liquid Mixture in
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EXERCISE 11 Synthesis of Aspirin (Acetylsalicylic Acid from Salicylic Acid) RAQUID‚ Rency J Group 5 18L I. Introduction Due to the demand of certain reagents in the laboratory in order to perform and conduct further experiments or produce essential compounds‚ chemists continuously develop organic synthesis. This process aims to prepare and synthesize desired organic compounds from commercially or readily available ones by providing the simplest route in synthesizing the compound
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being unsaturated‚ would be expected to react like typical olefinic compounds. But this is not the case‚ for example: 2 Br Br2 Br2 CCl4 CCl4 Br No reaction BUT OH KMnO4 - KMnO4 - OH No reaction OH OH Conclusion: Benzene is stable to both Br2 / CCl4 and KMnO4 / -OH. Therefore‚ there is something unusual about the double bonds in benzene‚ the unsaturation is atypical / unique 2. Benzene undergoes substitution rather than addition reaction‚ i.e.‚
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OBJECTIVES: To determine the maximum wavelength of potassium permanganate. To plot the calibration curve of potassium permanganate. To determine the concentration of an unknown solution of potassium permanganate. INTRODUCTION: UV Spectrophotometer has 4 main components which is the UV light source‚ the sample‚ detector and the processor/recorder. Spectrophotometry is a technique that uses the absorbance of light by an analyte (the substance to be analyzed) at a certain wavelength to determine
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of this experiment is to determine the rate of a chemical reaction (potassium permanganate‚ KMnO4‚ + oxalic acid‚ H2C2O4) as the concentrations are varied and to determine the rate law for the reaction. Since rates depend on temperature‚ we will also look at the effect of temperature on the rate of this reaction.The reaction rate or the oxidation-reduction between oxalic acid and potassium permanganate‚ KmnO4 is measured by recording the time elapsed for the purple colour of the permanganate ion to
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three clean dry labeled 125 mL erlenmyer flasks on an analytical balance. Place about 0.135 grams of oxalic acid dihydrate‚ H2C204.2H20‚ into each of the three separate flasks and reweigh the flasks containing the acid. (2) Set up a buret with KMnO4 solution to be standardized by titration. (3) Dissolve each acid sample in about 25 mL of distilled water. Again don’t mix up the samples. Take one flask and add 1-2 mL of concentrated sulfuric acid. · CAUTION! Concentrated sulfuric
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Table 4. Factors that affect reaction rates You’ll be studying various aspects of kinetics of three reactions. A. Reaction between lead nitrate (PbNO3) and potassium chromate (K2CrO4) solutions B. Reaction between potassium permanganate (KMnO4) and oxalate ion (C2O42-) C. Iodine clock reaction A. REACTION BETWEEN LEAD NITRATE AND POTASSIUM CHROMATE SOLUTIONS Lead nitrate reacts with potassium chromate to form yellow lead chromate precipitate and aqueous potassium nitrate. The formation
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Alkane‚ Alkene‚ Alkyne & Aromatic Learning Objectives 1. 2. 3. Determine the IUPAC name‚ common name and structure of an alkanes‚ alkenes and cycloalkanes. Identify the physical properties of alkanes. Describe briefly natural sources and importance of alkanes Describe reactions of alkanes Propose a mechanism on free radicals substitution 4. 5. 6. Describe the preparation and reactions of alkenes. 7. Propose mechanism on preparation; dehydration of alcohol 8. Define carbocation
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