Introduction In this experiment‚ the essential oil eugenol (the main component of oil of cloves) will be isolated from whole cloves using the technique of simple distillation‚ which is often used to isolate liquid natural products from plants. The mixture of whole cloves and distilled water will then be heated to boiling and the distillate (a eugenol/water mixture) will be collected. The eugenol will then be separated from the water by extraction with pentane. The pentane solutions will then be
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Laboratory #16: Analysis of Grease in Water by Solvent Extraction Experiment Date: 2/19/10 Due Date: 2/26/10 II. Objective The goal of this lab was to determine the amount of impurity‚ in the form of oil‚ in water using the method of solvent extraction‚ also known as liquid-liquid extraction‚ a method of separating two materials with different physical and/or chemical properties. Two methods of evaporation will be used to finally determine the concentration of impurity- one using an explosion-proof
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transesterfication and direct esterification routes‚ respectively. Since its commercialization in the 1950’s by DuPont‚ PET was predominantly synthesized out of DMT due to the fact that this monomer‚ compared to TPA‚ was relatively easily purified by distillation. Yet‚ since the 1960’s‚ purified TPA became available by the development of new technologies and gained a lot of importance as a monomer in polyester synthesis (Matsuzawa‚ K.‚ 1976). The applications for PET include fibres and filaments‚ films
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useful to make cinnamic acid. Experimental Section This experiment was performened on a 40 mmol scale. The materials we will use will be salicylaldehyde‚ Ethyl acetoacetane‚ Piperidine and Ethanol. In a 150ml single-neck round bottom flask equipped with a stir bar‚ add salicylaldehyde. We used 4.89g or one equivalent. Then add ethyl acetate to the round bottom flask. We added 5.47g or 1.05 equivalent. Add 40 mL of ethanol to the round bottom flask make sure to stir. While stirring add the piperidine
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POLYMER DATA HANDBOOK *Home *Browse/Search Contents *Browse by Polymer Class *Browse the Index *Online help Copyright © 1999 by Oxford University Press‚ Inc. EDITED BY JAMES E. MARK‚ UNIVERSITY OF CINCINNATI PUBLISHED BY OXFORD UNIVERSITY PRESS The online version of the Polymer Data Handbook includes key data on over two hundred polymers. Please note that entries are presented as PDF files and can only be read using Adobe Acrobat Reader Version 3. If you do not have the freeware reader‚
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HPTLC and 0.05g of the crystallised product above was placed into a sample vial which contained 1cm3 of ethyl acetate solvent shaken and dissolved. This sample of synthesised solution and a further two other solutions of pure paracetamol and 4- aminophenol solution sample were separately loaded by capillary action in different positions. These were then placed in a jar containing ethyl acetate (2cm3) and the results were visualized under the UV
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component mixture by extraction 4. Completion of experiments from day 1 to 4 5. NMR workshop 6. Sandmeyer Reaction: Preparation of p-chloronitrobenzene 7. Synthesis of benzilic acid from benzil 8. Aldol Condensation: Preparation of ethyl cinnamate 9. Isolation of caffeine from tea 10. Completion of isolation of caffeine from tea 11. Catchup day and completion of experiments School of Chemistry University of KwaZulu-Natal‚ Westville Campus OCCUPATIONAL
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Dictionary of chemical formulas From Wikipedia‚ the free encyclopedia This is a list of chemical compounds with chemical formulas and CAS numbers‚ indexed by formula. This complements alternative listings to be found at list of inorganic compounds‚ list of organic compounds and inorganic compounds by element. Table of contents: A B C Ca-Cu D E F G H I K L M N O P R S T U V W X Y Z & [edit] Tables to be merged Inorganic: A B Ca-Cu G H I L M N O P S Organic: C C2 C3 C4 C5 C6 C7
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CH3COOH Assay of Aspirin capsules Aqueous Alkalimetry Residual titration 0.1N NaOH Phenolphthalein TS C6H4OCOCH3COOH + NaOH C6H4OCOCH3COONa+ H2O Assay of Metacholine Chloride Non Aqueous Acidimetry Blank titration Perchloric acid Mercuric acetate TS Crystal violet TS 2 Cl- + Hg (OAC)2 + 2HClO4 2 ClO4- + 2HOAc + 2HgCl2 Assay of Phenytoin Non Aqueous alkalimetry Blank titration Sodium methoxide Saturated sol’n of Azo violet in Benzene H C6H5 N--C=O
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This page intentionally left blank SEPARATION PROCESS PRINCIPLES Chemical and Biochemical Operations THIRD EDITION J. D. Seader Department of Chemical Engineering University of Utah Ernest J. Henley Department of Chemical Engineering University of Houston D. Keith Roper Ralph E. Martin Department of Chemical Engineering University of Arkansas John Wiley & Sons‚ Inc. Vice President and Executive Publisher: Don Fowley Acquisitions Editor: Jennifer Welter Developmental Editor:
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