Colegio de San Juan de Letran College of Liberal Arts and Sciences Experiment #3 SEPARATION AND PURIFICATION OF ORGANIC COMPOUNDS: CRYSTALLIZATION Gomez‚ Paola Anne M. DOP: 2 July 2013 Student no. : 4120403 DOS: 9 July 2013 Group: Carcinogenic Remarks: _____________________________________________________________________ Engr. C. D. Sanchez Instructor THEORETICAL DISCUSSION Crystallization is a technique which chemists use to purify solid compounds. It is
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Abstract: The objective of the experiment was to prepare Benzilic acid by multistep synthesis starting with benzaldehyde. In this setup however‚ product of the first step‚ Benzoin‚ is provided thereby omitting the first step involving the conversion of benzaldehyde. For this experiment‚ the microscale techniques of reflux‚ crystallization‚ and melting-point determination were used. Utilizing these techniques a product yield of 93% for benzil and 57% for Benzilic acid was obtained‚ as well as
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PRINCIPLES OF CHEMISTRY LAB I Experiment 2 Separation Of Mixtures INTRODUCTION A mixture can simply be defined as a substance that is made up or consists of two or more elements and/or compounds that are physically combined but that have not reacted chemically to form new substances. A mixture may be a solid‚ liquid‚ gas‚ or some combination of those states. Mixtures can be found almost every wher in our everyday lifes and some common examples are * sand and water * salt and water
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Introduction: In the lab‚ Bromide was combined with trans-cinnamic acid in order to see if the resulting product at the end of the experiment would yield either an erythro- or threo-dibromide. Based on how well this experiment was done there is a possible product that would have a melting point around 95°C‚ threo-‚ 205°C‚ erythro-‚ or somewhere in the middle which would be a combination of the two. The process of refluxing was used to purify the mixture followed by crystallization. In the end
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Purposes of Experiment: To synthesize a transition metal complex‚ potassium tris (oxalate)ferrate(III) trihydrate in a two step process‚ to learn new laboratory techniques such as decantation‚ recrystallization‚ gravity and suction filtration. Also the purpose of the experiment is to determine the actual‚ theoretical‚ and percent yields of product‚ and characterize the final compound by determining the number of waters of hydration by gravimetric analysis List of Observations: After adding
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Introduction Aromatic compounds‚ which are planar cyclic rings with (4n+2)π electrons‚ will not undergo simple addition reactions like those of alkyl substances. However‚ in the presence of an electrophile‚ aromatic compounds will undergo electrophilic aromatic substitution. In this type of reaction‚ two π electrons from the aromatic ring serve for the ring to act as a nucleophile and attack an electrophile. For nitration‚ this nucleophile is NO2+‚ which is produced by reacting nitric and sulfuric
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Chem 3650 Organic II Lab Lecture Summer 2013 Instructor: Victoria Dougherty M.S. Victoria Dougherty M.S. Office: BSE 1.340 Phone: 458-5473 (I do not have voicemail) Office Hours: Tuesday and Thursday: noon – 1:00 pm (or by appointment) Monday and Wednesday: 1:00 pm to 2:00 pm E-mail: victoria.dougherty@utsa.edu (put Chem 3650 in subject) Lab instructors and sections: Lab instructors Email (put Chem 3652 in subject) Section(s) Times Marilyn Wooten PhD. marilyn.wooten@gmail.com 01T 7:30–11:20
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Over 40% of medicinal chemicals in the world were developed from isolation of the natural source. These sources were from fungi‚ plants‚ bacteria‚ animals‚ etc. The techniques used to isolate and purify has been by extraction‚ distillation‚ recrystallization‚ and chromatography. In this experiment we will be trying to obtain a pure organic compound from a natural source. Because this natural source it is not only trimyristin and myristic acid that makes it up‚ it’s a mixture of many compounds. Although
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From the research‚ it is clear that a big emphasis has been placed on the search for life and the characterization of geological Martian substances. To add to this‚ the purpose of this mission is to locate evidence of current of past life underground and to test the ability of Mars to sustain life. Using the research conducted in past‚ current‚ and future Mars missions‚ this mission proposes three questions about Mars that correlate to the Mars Exploration Program (MEP) science goals and guide the
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product. Procedure: Schoffstall‚ A.M.‚ Faddis‚ B.A.‚ and Durelinger‚ M.L. Microscale and Miniscale Organic Chemistry Laboratory Experiments‚ 2nd Ed.‚ McGraw-Hill‚ 2004‚ pages 215-218. Experiment 12.2 A Changes: Part A- No methanol recrystallization. Results and Observations * all literature values were obtained at www.sigmaaldrich.com Chemical Volume (mL) Mass (g) Density (g/mL) Molecular Weight (g/mol) Methyl-3-nitrobenzoate - 0.1178
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