"Synthesis of salicylic acid and potentiometric determination of its purity and dissociation constant" Essays and Research Papers

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    Introduction This lab’s purpose was to determine whether Salicylic Acid made from methyl salicylate is the same as Salicylic Acid made from benzene. This information can be found by comparing the difference in melting points of the two samples of Salicylic Acid. Here are the physical properties of Salicylic Acid and the mechanism of reactions that occurred in this lab. How Salicylic Acid is derived: Procedure/Results First‚ .26mL of 2.0mmol methyl Salicylate was measured and put

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    #15 Synthesis of Ethyl Salicylate from Salicylic Acid ____________________________________________________________ _______________ Purpose: Salicylic acid is converted to the liquid ethyl salicylate by addition of ethanol. Yields of salicylic acid (week 1) and ethyl salicylate will be found‚ as well as the overall yield of the 2-step conversion of acetyl salicylic acid to ethyl salicylate. Introduction: Esters are formed from the reaction of acids and alcohols: O O

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    Report Written: 08/02/2009 Synthesis of Acetyl salicylic acid (Aspirin) Abstract Introduction: The following report contains information on how to produce aspirin. The experiment has been carried out on a small laboratory scale. The experiment starts by combining such chemicals such as salicylic acid and acetic anhydride. The synthesis of aspirin is classified as an esterification reaction. This is a substitution reaction where the alcohol group from salicylic acid reacts with ascetic anhydride

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    Determination of Equilibrium Constants Introduction Bromothymol blue is an indicator for many acid-base titrations. When adding different solutions within the indicator it is to react and change colors‚ in this experiment the different colors were blue‚ green‚ and yellow. In the following experiment‚ obtaining the absorbance levels for each one makes it possible to calculate the equilibrium constant. Materials and Methods For this specific experiment there are a few materials that are crucial

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    Acetylsalicylic Acid (Aspirin) Synthesis Telow‚ AJV Sumicad‚ CJ‚ Tavanlar‚ EMMT‚ Chem 40.1‚ Institute of Chemistry‚ University of the Philippines Los Baños I. Introduction Organic synthesis is the process where a desired organic compound is constructed or prepared from commercially available materials. The objective of organic synthesis is to design the simplest synthetic routes to a molecule. Aspirin‚ also known as acetylsalicylic acid is as salicylate drug often used as analgesic

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    Determination of the Rate Constant for a Chemical Reaction Department of Chemistry Abstract This experiment was performed to determine the rate constant k‚ for hydrolysis of tertiary butyl chloride to tertiary butanol. The solvent system for this reaction is 45% isopropyl alcohol and 55% water. The rate of hydrolysis of t-butyl chloride is measured by the decrease in the concentration of this reagent with time. The rate of decomposition of t-butyl chloride must be equal to the rate of formation

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    October 9‚ 2013 Partner(s): Acetylsalicylic Acid Synthesis Theory. This experiment was carried out to see how the hydroxyl group on the benzene ring in salicylic acid reacts with acetic anhydride to form an ester‚ and to make aspirin. Synthesis of Acetylsalicylic Acid occurs by protonation of carbonyl (C=O) group‚ and a nucleophilic attack of OH on the acetic anhydride. The ferric chloride test and melting point were used to test the purity of the results. A hypothesized recovery rater of above

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    Ngoc Pham Chem162B Lab #2: Trends in Periodic Table Date: 01/10/2011 Lab partner: Ian Bauer Result Section: Table I: The solubility of the alkaline earth metal ions | SO42- | CO32- | C2O42- | IO32- | Mg2+ | S | I | S | S | Ca2+ | I | S | S | I | Sr2+ | S | S | S | I | Ba2+ | I | I | I | S | Key: I- insoluble‚ S-soluble Table II: Color of water (Halide) and Halogen (Hexane) layers | Cl2 | Br2 | I2 | Hexane layer | Clear | orange | Pink | Water layer | Clear‚

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    Determination of an Equilibrium Constant Abstract: In this experiment‚ two reactions were run to determine the molar absorptivity and the equilibrium constant of FeSCN2+. The main principles used in this lab are equilibrium‚ LeChatlier’s Principle‚ Beer’s Law and Spectrocopy. The first reaction was run to completion using LeChatier’s Principle and the second reaction was run to equilibrium. A spectrophotometer was used to measure absorbances. Using a graph of absorbance versus concentration

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    DETERMINING THE EQUIVALENT MASS AND DISSOCIATION CONSTANT OF AN UNKNOWN WEAK ACID BY TITRIMETRY INTRODUCTION Acids are substances that donate hydrogen ions and bases are substances that accept hydrogen ions. Acids and bases react with each other by transferring hydrogen ions. One way to distinguish an acid is by its equivalent mass‚ which is the number of grams of the acid needed to transfer one mole of hydrogen ion to a base. For a monoprotic acid‚ which only transfers one hydrogen ion‚ its

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