“The Synthesis of Zinc Chloride”‚ what a peculiar name for a lab that does not even involve synthesis. Synthesis‚ by definition‚ is when two elements are combined in a chemical reaction‚but that is not the case. In this lab we are combining zinc‚ an element‚ and hydrochloric acid‚ a compound‚ but combining a compound and an element is not synthesis‚ it is single replacement. We are taking zinc and hydrochloric acid and making zinc chloride and hydrogen‚ a single replacement‚ but what occurred during
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CHEM 1474-E01 Chemistry for Everyday WEEK5 Lab Report Spring 2017 Instructor: Kyoung Nan Kim Office: SI3076 Email: kyoung.kim@ucdenver.edu Office hour: M/W 1:00p-2:30p (SI3076) T/Th 12:30p-1:30p (SI3076) • All communication should be done via school email (xxxx@ucdenver.edu) • The work will be submitted through canvas assignments. You can simply upload doc/pdf files under “Lab report” assignment tap. • Review: Ch2‚ Ch3.5‚ Ch 4.2‚ Ch6.1 and Ch7.1-Ch 7.3 in your text book (21st
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The structure and synthesis of TPC is outlined in Scheme 1. Briefly‚ the compound 1 was synthesized as per literature procedure. 2 was synthesized by reacting 1-methy pyrazole-4-boronic pinacol ester with 1 by suzuki-coupling‚ the final product TPC was synthesized by treating with malononitrile in the presence of piperidine as a base and ethanol as solvent. The detailed synthesis procedure given in the experimental section. The structure and purity of TPC was unambiguously confirmed by 1H and 13C
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the gravity filter and the Hirsch funnel‚ as it was difficult to obtain the entire product from the filter paper and the sides of the funnel. As the experiment follows a semi microscale technique even a small amount of lost product yields a great loss in the yield 4. These sources of error could be minimized by doing a larger reflux in order to increase the yield. However‚ as the purpose was to simply synthesis SnI4 in order to identify the stable oxidation states (the melting point range requires
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The lipase gene sequence from Alcaligenes sp. JG3 was translated into amino acid sequence using two methods‚ manual translation and ExPASy online software. By manual method‚ amino acid sequence was obtained via codon translation one by one as shown in Figure IV.7. The sequence reference used is the lipase from A. faecalis MOR02 due to having high similarity with the lipase sequence from strain JG3 during CLUSTAL alignment and the alignment of the deduced amino acid with the referred sequence was
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The first step was to prepare 400 mL of an 0.1 M solution of NaOH. This was done by diluting from the 6 M solution that was provided. Next‚ 0.715g of KHP was weighed using the glazed paper and the triple beam balance. The KHP was then transferred to the 250 mL Erlenmeyer flask. Using a graduated cylinder‚ 50 mL of deionized water was measured and added to the flask. The KHP was dissolved in the water‚ and few drops of phenolphthalein were added. Moreover‚ the burette was rinsed with deionized water
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Every cell‚ whether it belongs to a plant‚ bacteria or a human‚ requires energy from varying food sources to survive. However‚ when cells break down food into its sugar components‚ i.e glucose‚ they cannot use the components directly because glucose holds a lot of energy it would be inefficient to use for reactions that don’t need a lot of energy. Imagine you want to buy pencils for $5 from a store that won’t give change‚ it is more economical to use a $5 or $10 bill than a $100‚ that way there is
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The purpose of the first week experiment was to determine the effect of Nitrophenyl phosphate concentration‚ the substrate‚ on the enzyme‚ acid phosphatase‚ reaction. In an enzyme reaction‚ there is substrate that binds to the active site of the enzyme and product is the end result. The enzyme is the catalyst for the reaction which means that it speeds up the process. Without enzymes‚ the majority of reactions would not occur because the activation energy level would be unattainable. With this in
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PRE-LAB The purpose of the lab is to determine the moles of hydrogen gas and then molar mass of the metal. First‚ the metal assigned to each group must be weighed out in order to ensure the hydrogen gas produced will not exceed the capacity for the gas measuring tube. Then‚ copper will be wrapped around the metal leaving 6-8cm at the end for a handle. The end wire will be bent into a hook to keep the sample at the bottom of the tube and increase the oxidation rate. A ring stand will need to be
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Lab #28 Conservation of Mass Ashleigh Bublinec Serena Contreras
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