Synthesis of benzilic acid from benzoin utilizing a multi-step reaction. Names: Arian Karim TA Name: Sayantan Das Lab Day & Time: Thursday 7:30-11:40 Lab Section #: Abstract The main purpose of this experiment was to synthesize benzilic acid from benzoin. This requires a multistep synthesis with benzyl as an intermediate product. The first step required HNO3 as an oxidizing agent and the second step required KOH and HCl. The percentage yields of benzil and benzilic acid were 59.5%
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What I found from my data proves my hypothesis to be correct. Since HCL has already a wide amplitude of ions‚ where the addition of sodium chloride just increases the overall ions in the solution‚ hence more conductivity; since electrons are moved through ions. What
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Results: For the solutions acid and bases lab the results my group received are as followed. Procedure 5.1 were we had to measure the ph of the following substances Vinegar 4 Apple Juice 4 Black coffee 5 Baking Soda + Sprite 8 0.01mM HCl 4 0.1mM HCl 3 Distilled water 4.5 Tap Water 5 Procedure 5.2 -Test the ability of buffers Before Buffer After Buffer Water 4 Water 4 0.1M phosphate buffer 6.5 0.1M Phosphate buffer 6.9 0.1M NaCl 4 0.1M NaCl 4.8 Procedure 5
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Kong Acid rain on plant -Background information Unpolluted rain is normally slightly acidic‚ with a pH of 5.6. Carbon dioxide (CO2) from the atmosphere dissolves to form carbonic acid. Acid rain is rain that has been made acidic by certain pollutants in the air. Acid rain is a type of acid deposition‚ which can appear in many forms. Wet deposition is rain‚ sleet‚ snow‚ or fog that has become more acidic than normal. Dry deposition is another form of acid deposition‚ and this is
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synthesised is only 67%-70% and a maximum 70% yield of ester usually is not considered to be acceptable for a synthesis reaction‚ instead it is considering as a poor yield of ester. The synthesised ester can only have a maximum yield of 70% because for ester in which the carboxylic acid and alcohol are sterically unhindered‚ a same ratio mixture of carboxylic acid and alcohol can only synthesis ester with a maximum yield of 70% ester as the reaction with the same ration of mixture will reach a state
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includes boronic acid and a halide that are catalyzed by a palladium complex under basic conditions. Other palladium- catalyzed coupling mechanisms include the Heck and Stille reactions. Palladium typically exists in the oxidation states of 0‚ +2‚ and +4. PdCl2 is usually the starting compound for several other heterogeneous palladium catalysts such as Pd/C and Pd/BaSO4.1 Suzuki coupling is an efficient way to
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(Fe3+ ) form. Ferric form is not usually absorbed in the body. In the stomach‚ there is low pH of 2 due to presence of gastric acids such as Hydrochloric and Ascorbic acids. These acids provide an acidic environment for reduction of ferric iron to ferrous (Fe2+). Ferrous iron can be absorbed in the body system. As in following equation of iron (iii) reaction with Ascorbic acid ‚ the product is iron (ii) chloride which is soluble 2 Fe3+ (s) + C6 H8 O6 (aq) → 2 Fe2+ (aq) + C6 H6 O6 (aq) + 2 H (aq)+
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The Grignard Synthesis of Triphenylmethanol Abstract: Grignard synthesis of triphenylmethanol was achieved by use of the Grignard reagent phenyl magesium brominde. The organometallic grignard reagent was synthesized by use of a reflux apparatus recrystallization techniques. Once synthesized it was used in a Grignard reaction that involved nucleophilic addition to a carbonyl in order to make triphenylmethanol. The final product was solidified and recrystallized and spectral data was
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EXERCISE 11 Synthesis of Aspirin (Acetylsalicylic Acid from Salicylic Acid) RAQUID‚ Rency J Group 5 18L I. Introduction Due to the demand of certain reagents in the laboratory in order to perform and conduct further experiments or produce essential compounds‚ chemists continuously develop organic synthesis. This process aims to prepare and synthesize desired organic compounds from commercially or readily available ones by providing the simplest route in synthesizing the compound
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of which RNA helps in the making of Protein‚ Translation is located in the Cytoplasm‚ and DNA is not involved in Translation‚ the ending result of Translation is the production Amino Acids‚ in Translation‚ tRNA and Ribosomes work together to make Proteins‚ Translation is when mRNA connects with tRNA but the Amino Acids information code is the 3 nucleotides bases in the mRNA code‚ the nucleotides that are in tRNA are Adenine‚ Uracil‚ Cytosine‚ Guanine‚ those 4 nucleotides never change‚ The mRNA and
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