nitronium ion NO2+. It then acted as strong electrophile that nitrated the benzene ring. After that‚ vacuum filtration and recrystallization were methods used to obtain the final product with minimal impurities. The mass of product
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Abstract: In this experiment‚ the methyl nitrobenzoate was prepared from methyl benzoate‚ concentrated HNO3‚ and concentrated H2SO4 via an electrophilic aromatic substitution reaction. The HNO3 and H2SO4 were combined to form a nitrating solution‚ which was mixed with a mixture of methyl benzoate and H2SO4. Percent yield for the final product was calculated followed by recrystallization and melting point was measured. Introduction: Nitration of Methyl Benzoate is one of the examples
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formula would be C8H11N with a HDI of 4. Looking at the IR spectroscopy‚ there is a sharp peak at around 3000 cm-1‚ which indicates C-H bonds. At around 1600 cm-1‚ we see a peak which tells us there are C=C that might corresponds to an aromatic benzene ring‚ which I proved using the NMR. The Nitrogen is also present on the IR spectroscopy leaving its mark with a peak at around 3200 – 3500 cm-1. Lastly‚ I finalized my structure using the NMR spectroscopy. With the information I have collected and
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Lab 6: Electrophilic Aromatic Substitution(1) Nitration of Methyl Benzoate(2) Synthesis of 1‚4-Di-t-butyl-2‚5-dimethoxybenzene byFriedel-Crafts Alkylation of 1‚4-DimethoxybenzenePurpose1)To carry out the nitration of methyl benzoate‚ and then identify the major product formed (position at which nitro-group substitution takes place) by thin-layer chromatography (TLC)‚ the percent yield and the melting point range. 2)To synthesize 1‚4-Di-t-butyl-2‚5-dimethoxybenzene by Friedel-Crafts Alkylation of
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Phenols You can prepare phenols in large quantities by the pyrolysis of the sodium salt of benzene sulfonic acid‚ by the Dow process‚ and by the air oxidation of cumene. Each of these processes is described below. You can also prepare small amounts of phenol by the peroxide oxidation of phenylboronic acid and the hydrolysis of diazonium salts. Pyrolysis of sodium benzene sulfonate In this process‚ benzene sulfonic acid is reacted with aqueous sodium hydroxide. The resulting salt is mixed with solid
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Analysis of Hydrocarbons Jovellanos‚ Bien Jindrich Johannes; Lacson‚ Danise Angelica; *Lagula‚ Nina Francesca; Lañez‚ Kristine Department of Psychology College of Science University of Santo Tomas España Manila 1015 Abstract A hydrocarbon is strictly composed of carbon and hydrogen atoms only. Five hydrocarbons were used namely hexane‚ cyclohexene‚ toluene‚ naphthalene (in hexane)‚ and the unknown (which will be known through parallel chemical tests). Three tests‚ nitration test‚ bromine
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Title : Properties of hydrocarbon Objective : 1) To study the properties of hydrocarbons. 2) To determine the unknown samples. Results : Part A : Combustion Compounds Observations Hexane There was orange flame and burned mildly during the burning process. No soots and smoke were produced. C6H14 + 19/2 O2 6CO2 + 7H2O Cyclohexene Orange flame burned vigorously. A small amount of black soot and smoke were produced during the burning process.
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group into something - in this case‚ into a benzene ring. The most commonly used acyl group is CH3CO-. This is called the ethanoyl group. In the example which follows we are substituting a CH3CO- group into the ring‚ but you could equally well use any other alkyl group instead of the CH3. The facts The most reactive substance containing an acyl group is an acyl chloride (also known as an acid chloride). These have the general formula RCOCl. Benzene is treated with a mixture of ethanoyl chloride
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ABSTRACT: The electrophilic aromatic substitution reaction is the attack of a benzene ring on an electrophilic species resulting in the substitution of a proton with a functional group. The electrophilic aromatic substitution reaction nitration is used to nitrate methyl benzoate and acetanilide with a nitronium ion. Crystallization was used to purify the product. The melting point was used to determine its purity and the regiochemistry of the products. The methyl benzoate reaction product‚ methyl
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UOP Linear Alkylbenzene (LAB) Complex Petrochemical Petrochemical Introduction Linear alkylbenzene (LAB) is the most common raw material in the manufacture of biodegradable household detergents. LAB is produced using normal paraffins as a raw material. Normal paraffins are derived from straight run kerosene. UOP offers processes‚ catalysts‚ adsorbents and equipment for the production of LAB from kerosene or normal paraffins. The processes can be utilized in combination in a new complex
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