Experiment A Volumetric Analysis A titrimetric analysis requires the careful addition of titrant. • To prepare and standardize a sodium hydroxide solution • To determine the molar concentration of a strong acid Objectives The following techniques are used in the Experimental Procedure Techniques 2 4 16b 16a 90 80 5 16c 6 13c 15a 15b ! A chemical analysis that is performed primarily with the aid of volumetric glassware (e.g.‚ pipets‚ burets‚ volumetric
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1.0 Calibration of Volumetric Glassware 1.1 Introduction: Calibration is the process by which a stated measure such as the volume of a container is checked for accuracy. In general‚ measurements of mass can be determined more precisely and accurately than measurements of volume. Therefore‚ the mass of the liquid contained or dispensed by the glassware will be measured and the corresponding volume calculated using the density of the liquid. However‚ a relatively small change in temperature
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VOLUMETRIC ANALYSIS 1. In volumetric analysis‚ the volume of a reagent needed to react with analyte is measured. 2. In a titration‚ increments of the reagent solution -the titrant-are added to the analyte until their reaction is complete. 3. The most common titrations are based on: - acid-base - oxidation-reduction - complex formation and - precipitation reactions 1. Methods of determining when the analyte has been consumed include: - detecting a sudden change in
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obtain a dry 10 mL volumetric flask that includes a stopper with it and weight on a digital scale. Be sure to get the mass at the closest milligram. Then‚ pour DI water to the calibration mark of the flask. Place the stopper back and weigh it again on the same digital scale. Once recorded‚ it is okay to pour this water down the drain. Observations: Mass of Empty Flask Mass of DI Water Filled Flask 15.114 g 25.048 g Now‚ put 100 mL of ethanol in a beaker and utilize a disposable pipet to fill the volumetric
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Experiment 2 CALIBRATION OF A PIPETTE Introduction An ordinary laboratory pipette may be expected to deliver its nominal volume with good precision and good accuracy if it is used in the way recommended. In this experiment we investigate the precision and accuracy of such a pipette by making accurate determinations of the mass of water it delivers in repeated operations. Materials 10.0-cm3 pipette‚ 50-cm3 beaker‚ thermometer‚ pipette filler‚ graph paper. Procedure
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The first flask was placed under a buret. Finally we titrated the KHP by adding the base until the end point was reached‚ which was when it turned pink completely. We repeated this twice and then cleaned up. The procedure does not include very difficult math‚ however the calculations did. The harder math calculations included finding moles of the acid‚ moles of the base that was used to neutralize‚ and the molarity of the base. After all calculations‚ below is what we concluded. The molarity you
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NO | ANSWER | MARK | 1 :( i )( ii ) ( iii ) ( iv )2 :( i )( ii )( iii )3 )4 )5 ) ( i )( ii )( iii )( iv )6 )7 ) i )ii ) iii )8 )9 )10 )i ) ii )iii)11 ) | A reagent is highly serves as a reference material in all volumetric & mass titrimetric method.A reagent solution of accurately known concentration. * End point-point at which the reaction is observed to be complete and there is permenant colour change at the end of titration. * Equivalent point-point at which an equivalent amount of
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Experiment 9 and 10: Volumetric/Vinegar Analysis Abstract: The goal of the experiment that was conducted was to figure out both the molar concentration of NaOH and the standard mole ratio of the NaOH solution. In order to find the concentration of the NaOH solution‚ volumetric analysis was used. In volumetric analysis‚ a titration mechanism was utilized in order to find the reaction that the base will end up having with KHC8H4O4
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Floyd Askew 3/19/13 CHEM 1211L Lab Report Introduction The purpose of this lab is to use volumetric analysis to determine the concentration of unknown substances. A sodium hydroxide solution is standardized to assist in finding the concentration of an acetic acid. An indicator must be used to pin point the equivalence point‚ the point in which 1 mole of a substance is equal to 1 mole of another. When that is found‚ we can determine the concentration. HC2H3O2 (aq) + NaOH (aq)
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Objective: Find the percentage of iron in a given sample through titration. EDTA CONCENTRATION 0.02060 M Mass of Ferric Salt 1.8193 g Burette Readings ( in mL) Trial 1 Trial 2 Trial 3 Final 42.19 21.29 39.69 Initial 23.35 2.61 21.21 Endpoint Volume 18.85 18.6 18.47 Average of the endpoint volumes V= 18.64 mL % Fe ± Sv 11.78% ± 0.19313 Calculations: sV= {[(v1 – V)^2 + (v2 – V)^2 + (v3 – V)^2]/2}^(1/2) {[(18.85 – 18.64)^2 + (18.6 – 18.64)^2 + (18.47
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