it comparison with literature though Melting point‚ TLC‚ IR‚ 1H and 13C NMR Abstract: The synthesis of the product: β-D-glucose pentaacetate is done though the acetylation using acetic anhydride with D-glucose with the help of sodium acetate. The recrystallization of the product is done though a polar solvent like water. The Result of this experiment has a percentage yield of 61% and analytical methods that are to detect the products are 1H NMR‚ 13 C NMR‚ COSY‚ FTIR (IR)‚ Thin Layer Chromatography
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under heat reflex. Purification and analysis will preform‚ by a simple distillation process. 21.44 g of banana oil will be used at the beginning. The liquid distillation occurs when the temperature reaches between 132-143 C‚ collect all the liquid in the vial after the temperature reaches this point. Last record the gas chromatogram in order. Conclusion: During this experiment‚ the product that condensed during the distillation process was 10.08 g in the first flask and 9.08 g in the second flask
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Grading System 2012-13 CM- 601 – Process Equipment Design - I Unit I Mechanics of materials: Stress- Strain relationships of elastic materials subjected to tensile‚ compressive and shear forces‚ Elastic and plastic deformation‚ General design considerations; Design of shell‚ bottom plates‚ self supported‚ and column supported roofs‚ wind girder‚ nozzles and other accessories. Unit II Unfired pressure vessel: Pressure vessel codes‚ classification of pressure vessels‚ Design of cylindrical and
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peaks (>10%) corresponding to methyl (triphenylphosphoranylidene) acetate‚ acetone‚ ethyl acetate‚ and hexane were identified. The phosphonium ylide peak indicates that the reaction did not go to completion (leftover starting material). Meanwhile‚ the acetone‚ ethyl acetate‚ and hexane peaks show there was residual solvent in the sample submitted for NMR analysis (compounds were not in reaction scheme). Because acetone‚ ethyl acetate‚ and hexane are volatile‚ we deduced that our evaporation of the
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INTRODUCTION: Carboxylic acids are organic acids characterized by the presence of a carboxyl group‚ -COOH. This acid acts as a weak acid‚ which can react with a strong base. Carboxylic acids form hydrogen bonds with many water molecules and are more soluble with one to four carbon atoms. Also‚ it may have an R group that consist of hydrogen or an alkyl group that changes its water solubility. Carboxylic acids with low molecular weight have odor at room temperature and higher molecular weight
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solvent Ethyl Acetate C4H8O2 88.11 0.897 -83.6 oC 77.1 oC Slightly soluble in water (~8.3g/100mL‚ 20 oC)‚ very miscible with alcohol‚ ether‚ acetone‚ benzene. Hexane C6H14 86.18 0.6548 -95 oC 69oC Immiscible with water Dichloro-methane CH2Cl2 84.93 -97 oC 40 oC 1.325 Slightly soluble in water (~1.3g/100mL‚ 20 oC)‚ very miscible with most organic solvent. Hazard 1. Ferrocene is highly flammable and it is harmful if swallowed. 2. Acetylferrocene is highly toxic if swallowed. 3. Ethyl acetate
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Experiment C: Identification and Separation of Dyes by TLC Pre-lab Properties: Ethyl acetate‚ ethanol‚ silica‚ azobenzene‚ azulene‚ 4-(p-nitrophenylazo) resorcinol‚ methyl red‚ bromocresol green (solubilities in water and ethanol) Purpose: To identify compounds from an unknown mixture using TLC Up to 100% of missed points can be recovered from this lab Watch the video: http://www.youtube.com/watch?v=e99nsCAsJrw (MIT) TLC plates are near the main hood DO NOT BREAK CAPILLARY TUBES Keep spots small
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LabVIEW (Laboratory Virtual Instrument Engineering Workbench)‚ created by National Instruments is a graphical programming language that uses icons instead of lines of text to create applications. A LabVIEW program consists of one or more virtual instruments (VIs)‚ Virtual instruments are called such because their appearance and operation often imitate actual physical instruments. The objective of developing a virtual interface that acquires data from physical instrument (pH probe) used in the monitoring
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from: http://www.stenutz.eu/chem/solv6.php?name=methylene+chloride Webmaster Webmaster. (2013). 1 - Propanol. Retrieved from: http://www.stenutz.eu/chem/solv6.php?name=1-propanol Webmaster Webmaster. (2013). Ethyl Acetate. Retrieved from: http://www.stenutz.eu/chem/solv6.php?name=ethyl+acetate Webmaster Webmaster. (2013). Hexane. Retrieved from: http://www.stenutz.eu/chem/solv6.php?name=hexane Webmaster Webmaster. (2013). 2-Butanol. Retrieved from: http://www.stenutz.eu/chem/solv6.php?name=2-butanol
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can also remove residues from glass and porcelain and it can also remove super glue from the skin. Perhaps‚ acetone is very useful in our everyday lives. Acetone is also known to remove ball pen marks on fabrics and clothings. It has ethyl acetate that is said to remove ball pen stains. Most people accidentally rubs ball pen marks on their clothing on a daily basis. The study was done to find out if acetone is more effective and easier to remove ball pen marks on clothings or
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