being that Silica gel in TLC 2 was polar and the solvent ethyl acetate-hexane is non-polar it moved relatively with the solvent. The stationary phase in TLC 3‚ alumina is non polar and the solvent ethyl acetate is polar so from the ideal that polar does not attract non-polar benzophenone stick stronger to alumina non-polar rather than moving up with polar solvent ethyl acetate as it did in tlc2. 6. Ethyl acetate is polar and Ethyl acetate- hexane is nonpolar‚ use of polarity differences. Because
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dissolves like”‚ fluorene dissolves with the non-polar heptane and the polar fluorenone dissolves in the polar ethyl acetate solvent. This phenomenon was illustrated in class before the experiment‚ when it was pointed out why water will not dissolve fluorene‚ fluorenone‚ or transstilbene as readily as a nonpolar solvent such as heptane or toluene‚ or a polar eluent such as ethyl acetate. Those solvents have a much more similar structure to the solutes‚ whereas water’s structure is much different
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Oxidation of an Alcohol: Oxidizing Methoxybenzyl Alcohol to Methoxybenzaldehyde Using Phase-Transfer Catalysis PURPOSE OF THE EXPERIMENT Oxidize methoxybenzyl alcohol to methoxybenzaldehyde‚ using sodium hypochlorite as the oxidizing agent and tetrabutylammonium hydrogen sulfate as the phase-transfer catalyst. Monitor the progress of the reaction by thin-layer chromatography. BACKGROUND REQUIRED You should be familiar with extraction‚ evaporation‚ and thin-layer chromatography techniques
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|[pic] | | | | |UNIVERSITI TEKNOLOGI MARA | | | |FAKULTI KEJURUTERAAN KIMA | | | |CHEMICAL ENGINEERING LABORATORY III | | | |(CHE575)
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ABSTRACT Purpose: To evaluate the antifungal and cytotoxicity activity of four medicinal plants like Mystroxylon aethiopicum‚ Lonchocarpus capassa‚ Albizia anthelmentica and Myrica salicifolia. Methods: Microdilution method and brine shrimp lethality test were employed to evaluate antifungal and cytotoxicity of plant extracts. Results: Lonchocarpus capassa leaf extracts exhibited antifungal activity against tested fungal strains with MIC range of 0.78 – 3.125 mg/mL with LCLA extract inhibiting C
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will used to hold this extraction and 5 mL of ethyl acetate will be passed through SPE column‚ to obtain and remove the caffeine from the SPE column. A small one-armed Erlenmeyer flask containing 5 mL of ethyl acetate along with the compound caffeine‚ should be the result after using the SPE column
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Figure 3 Superoxide radical scavenging activity. Values are mean ± SEM (n = 3). ABL‚ lyophilized aqueous extract of A. bilimbi fruits; ABP‚ petroleum ether fraction of ABL; ABE‚ ethyl acetate fraction of ABL; ABB‚ butanol fraction of ABL; ABW‚ aqueous fraction of ABL; QU‚ quercetin. 3.3.5 Nitric oxide radical scavenging activity Lyophilized aqueous extract of Averrhoa bilimbi fruits (ABL) and its different solvent fractions exhibited a dose dependent inhibition of nitric oxide radicals. The IC50
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September 30‚ 2012 Experiment 5‚ Preparation of Synthetic Banana Oil Introduction: This experiment prepares synthetic banana oil (isopentyl acetate) through the Fisher esterification method by combining isopentyl alcohol with acetic and sulfuric acid then heating the mixture under reflux for an hour. Esterification is a chemical reaction in which two reactants (an alcohol and an acid) form an ester as the reaction product. Observations and Data: When the sulfuric acid was combined
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from the molecule by ionization: CH3CO2H → CH3CO2- + H+ Because of this release of the proton (H+)‚ acetic acid has acidic character. Acetic acid is a weak monoprotic acid. In aqueous solution‚ it has a pKa value of 4.75. Its conjugate base is acetate (CH3COO−). A 1.0 M solution (about the concentration of
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crushing the seeds‚ then placing them into a distillation apparatus. The distillation apparatus evaporated the liquid from the seeds‚ which was captured in a flask. Next‚ DCM was added to the distillate‚ which allowed the water to be separated from the anise oil. Finally‚ the DCM evaporated and the pure anise oil was collected. The process of steam distillation allowed the anise oil in the seeds to be safely separated from the seeds. During the distillation process‚ water and crushed up seeds were
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