The intermolecular forces that can be present in a solution are london dispersion forces‚ dipole-dipole force‚ hydrogen bonding and ion-dipole forces. In this experiment the substances that were used were acetone‚ methanol‚ water‚ 1- butanol and ethyl acetate. Acetone is the organic compound with the formula (CH₃)₂CO. It is a colorless‚ volatile‚ flammable liquid‚ and is the simplest ketone. It takes 21 seconds for it to completely disappear. It was the first to evaporate among all tested substances
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aMicroscale Synthesis of Isopentyl Acetate (Banana Oil) Objective: Carried out the microscale synthesis of isopentyl acetate by direct esterification of acetic acid and isopentyl alcohol. This was an acid catalyzed Fischer esterification. Both extraction and distillation were employed to obtain a pure product. IR spectroscopy and gas chromatography were used to determine purity of the final product. Reagents: * Compound: | * MW (g/mol): | * MP (°C): | * BP (°C): | * Density (g/mL):
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solvents. However in this green chemistry experiment‚ a safer chromatography solvent mixture (hexanes and ethyl acetate) is used to help with the avoidance of solvent usage‚ the use of solid supported reactions and the use of alternative energy sources. Materials & Methods * 0.43ml of Benzaldehyde 0.30ml of pyrrole * 0.63g of Silica Gel 15ml of Ethyl Acetate * 25 mL Erlenmelyer flask Glass rod * Microwave oven Pyrex watch glass
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CHEMISTRY OF NATURAL PRODUCTS Terpenoids Sameena Bano Department of Chemistry Faculty of Science Jamia Hamdard New Delhi-110062 (24.09.2007) CONTENTS Introduction Classification of Terpenoids Isolation of mono and sesquiterpenoids General properties of Terpenoids General methods of structure elucidation Terpenoids Citral Menthol Camphor Eugenol Keywords Terpenes‚ isoprene‚ citral‚ menthol‚ camphor and eugenol 1 Introduction There are many different classes of naturally occurring
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sink drain but the other must go into the designated waste container. State of Sep Funnel Description Picture/Visual 20 mL of water and ethyl acetate with red dye separated by layer The red layer is clearly the bottom water layer since we know the dye was polar and supposed to mix / interact with the water layer. Therefore‚ the top layer must be the ethyl acetate
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concentration of the extract that scavenges 50% of the ABTS•+. The ABTS•+ scavenging abilities of the crude extract as well as the ethyl acetate fraction and its sub-fractions are presented in Table 2. For the solvent partitioned fraction‚ a similar trend to the DPPH• scavenging results was observed in the ABTS•+ scavenging activity‚ with the highest activity being found in the ethyl acetate fraction (IC50 = 61.0 _g/ml)‚ which was 3.7 times lower than those of the crude ethanolic extract (IC50 = 223.2 _g/ml)
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Allelopathic activity of the aqueous methanol extracts of Mangifera indica L. leaves The aqueous methanol extracts obtained from mango leaves inhibited seed germination of radish and sand fescue‚ and inhibited seedling growth of root and shoot growth of radish‚ rapeseed‚ sand fescue and crabgrass (Figure 1 and 2). The extract obtained from 0.03 g dry weight of mango leaves inhibited 20 and 50 % germination of radish and sand fescue respectively‚ on day 4 (Figure 2). The extract obtained from 0.03
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Preparation of Synthetic Banana Oil September 20th‚ 2012 Purpose: The main purpose of this experiment was to synthesize banana oil (isopentyl acetate.) Ester are often prepared by the Fischer esterification method‚ which involves heating a carboxylic acid with an alcohol in the presence of an acid catalyst. Theory: Synthesize isopentyl acetate by combining isopentyl alcohol with acetic acid and sulfuric acid and then heating the reaction mixture under reflux for an hour. The alcohol is the
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precipitate formed Formation of Esters a. From Carboxylic acids Acetic acid + ethanol + H2SO4 - produced a sweet smell b. From Acyl Halides Ethanol + H2O + H2SO4 - produced a sweet smell Hydroxamic acid test for the Ester group Ethyl acetate in ether + NH2OH.HCl + KOH heat effervescence + alcoholic HCl + FeCl3 – red colored solution Hydrolysis of acid derivatives H2O + Acetic anhydride 2-immiscible layer formed‚ blue litmus paper turned red‚ test tube becomes warm
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16 Application of TLC in the Isolation and Analysis of Flavonoids Marica Medi-Šari‚ Ivona Jasprica‚ c c Ana Mornar‚ and Željan Maleš CONTENTS Introduction ................................................................................................ 405 16.1.1 Chemistry‚ Biochemistry‚ and Medicinal Significance of the Flavonoids.......................................................................... 405 16.1.2 Brief Overview of Use of TLC in the Analysis of Flavonoids in Plants ........
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