From Gas to Rust: Measuring the Oxygen Content of Air Questions Why does the water level eventually stop rising? Materials Six measuring beakers 6 ring stands 2 clamps 750 milliliters of water 2.9 grams of steel wool 2.9 grams of copper 2.9 grams of iron Masking tape Permanent marker Procedures 1. Fill all six jars with water so that they are nearly full. It may be helpful to use a measuring cup to make sure that each jar has exactly the same amount of water
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Procedure 2.0 g of Mo(CO)6 and 10 mL of mesitylene were added into a 50-mL round bottom flask along with a small magnetic stir bar. A 30-cm reflux condenser was attached to the round bottom flask and a gas inlet was then connected to the condenser and to the bubbler. Since Mo(CO)6 and the product tends to react with oxygen at high temperatures this reaction must take place in an inert atmosphere. Therefore‚ the gas inlet was connected at the top of the condenser to a nitrogen source and was flushed
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The first step was to prepare 400 mL of an 0.1 M solution of NaOH. This was done by diluting from the 6 M solution that was provided. Next‚ 0.715g of KHP was weighed using the glazed paper and the triple beam balance. The KHP was then transferred to the 250 mL Erlenmeyer flask. Using a graduated cylinder‚ 50 mL of deionized water was measured and added to the flask. The KHP was dissolved in the water‚ and few drops of phenolphthalein were added. Moreover‚ the burette was rinsed with deionized water
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Weighed accurately about 25.0 mg of baclofen and transferred to 25 ml volumetric flask. Added 20 ml of a 0.001 M aqueous hydrochloric acid solution and sonicated to dissolve and degassed. The resultant solution diluted up to the mark with diluents to obtain 1000 μg/ml. Further stock solution was used to prepare plasma standards to construct the calibration curve. C. Pre-chromatographic isolation of baclofen from plasma Prior to chromatography‚ baclofen from plasma constituents was isolation by adding
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LAB 02: Measuring and Dispensing Liquids Introduction Pipetting is one of the most important and basic skills when it comes to experimental science. Good pipetting skills allow an individual to put trust in his or her results‚ prevent waste of materials‚ and assure reproducibility of results. In order to correctly pipette liquids‚ the volume range must be first determined. p1000 micropipettes have a volume range of 200 - 1000 uL‚ p200 micropipettes have a volume range of 20 - 200 uL‚ and p20 micropipettes
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Determination of an Unknown Concentration of Potassium Manganate using Colorimetry Introduction The purpose of this experiment is to conclude the concentration of an unknown solution using colorimetry to plot a calibration curve. Colorimetry measures the absorption of light at wavelengths within the visible region of the electromagnetic spectrum. It can be used to identify the unknown concentration of a solution in reference to a solution of a known concentration. When a solution appears
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Katie Smith April 11‚ 2013 Competitive Nucleophiles Introduction The purpose of this experiment was to compare the nucleophilicities of chloride and bromide ions toward the n-butyl and t-pentyl alcohols. We were able to analyze this by using refractometry to measure the amounts of alkyl chloride and alkyl bromide in each reaction. Experiment Scheme (Procedure A) To begin the experiment‚ we assembled a reflux apparatus in the fume hood with a 100 mL round bottom flask and a condenser
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Separating Acids and Neutral Compounds by Solvent Extraction Introduction The purpose of this experiment was to use solvent extraction techniques in order to separate a mixture consisting of a carboxylic acid (p-toulic acid)‚ a phenol (p-tert-butylphenol)‚ and a neutral compound (acetanilide). Extraction is the process of selectively dissolving one or more of the compounds of a mixture into an appropriate solvent‚ the solution that contains these dissolved compounds is called an extract (Manion
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Laurie Coleman Chem 3411 Dr. Eidell October 24‚ 2014 Preparation and IR Analysis of 2-chloride-2-methylbutane Line Reaction Abstract The purpose of this experiment was to react 2-methyl-2-butanol with concentrated HCl in order to form 2-chloride-2-methylbutane. The hydrogen for the HCl make the -OH from the 2-methyl-2-butanol into a good leaving group because H2O is formed. The H2O leaves and Cl- is free to bond with the carbocation creating 2-chloride-2-methylbutane. The materials needed
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Material and Methods * Osmosis : -thistle funnel tube -dialysis tubing sack -saturated NaCl w/food coloring -beaker with distilled H2O The experiments begins with the construction of a simple osmometer by obtaining pre-soaked length of tubing ‚opened and tied at the end. The tube is filled with saturated NaCl solution (with added food coloring) and the thistle is inserted in the dialysis tubing. The dialysis tubing is sealed to the thistle funnel with dental floss and placed in a beaker
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