cohesive energy density 1.5 Literature review 2. Experimental method 2.1 Solubility of SN 1010 in various solvents 2.2 Calibration curve 2.3 Preparation of polymer/antioxidant mix for films 2.4 Soxhlet extraction 2.5 Broadband dielectric analysis of films 2.6 Broadband dielectric analysis of molten samples 3. Results and discussion 3.1 Solubility of SN 1010 in various solvents 3.2 Calibration curve 3.3 Soxhlet extraction 3.4 Broadband dielectric analysis of films 3.5 Broadband dielectric
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A‚ B‚ and C are as follows: 68.6 %‚ 54.6 %‚ and 55.9 %. Introduction In the chemical process of bromination‚ an alkene is halogenated with bromine. Solvents that are typically used include methylene chloride and carbon tetrachloride along with iodine‚ the traditional reagent. However‚ because of the carcinogenic properties of the solvents and the corrosiveness of iodine‚ other alternatives are utilized : bromination with pyridinium tribromide‚ bromination with hydrogen peroxide and hydrobromic
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The Separation and Purification of Organic Compounds Sunshine Marie Introduction Each year‚ many thousands of new or unknown organic compounds are prepared or extracted from natural sources such as plants‚ fungi and animals. In order to identify an unknown organic compound or the components of a mixture of organic compounds‚ it is necessary firstly to separate and purify the compounds. At any given temperature‚ a certain number of molecules of a substance in the liquid state have sufficient
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fistula leaf were 15.2‚ 24.5‚ 43.8‚ 68.2‚ and 158.6 mg‚ respectively‚ with chloroform‚ petroleum ether‚ methanol‚ distilled water‚ and ethanol solvents. Evaluation of phytochemicals such as alkaloids‚ flavonoids‚ carbohydrates‚ glycosides‚ protein and amino acids‚ saponins‚ and triterpenoids revealed the presence of most of the constituent in polar extracts such as ethanol‚ methanol‚ and aqueous
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Compounds From Natural Sources: Extraction of Trimyristin From Nutmeg Introduction The purpose of this experiment is to illustrate how a solid natural product can be extracted from its natural source through the use of an organic solvent. Natural products are organic compounds that are synthesized by natural biological processes in plants‚ animals and microorganisms. These products typically occur in mixtures of many different compounds‚ so to obtain a particular natural product
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containing solvent of petroleum ether and acetone and chromatography paper stapled into a cylinder marked with a pencil line about 1cm from one end. An extract of chloroplast pigments where obtained and a blender was used to rupture the cells. Pigments were then extracted with acetone an organic solvent. Then pigment extracts were separated using paper chromatography. Pigment extract was applied to a cylinder of chromatographic paper then the cylinder was placed in a jar with the organic solvents.
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a solid to allow a crystal to grow. The method is when the solute in a hot solvent yields to a solution. Once the solvent cools‚ the solution is saturated with respect to the solute‚ which is when it recrystallizes. A crystal is the end result of the method and it is a single pure substance with the impurities being excluded from it. The recrystallization method can be broken down into seven steps: 1) Choosing the solvent‚ 2) Dissolving the solute‚ 3) Decolorizing the Solution‚ 4) Filtering suspended
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multiple techniques to complete and verify the bromination of trans-stilbene. First technique we used was to reflux the mixture; this contains having the mixture boiling so it will evaporate while the condenser will recondense the solvent which is boiling off so the solvent may stay in the reaction. Next we used the melting point of the product to verify which product was produced along with the purity of the compound. Lastly we did a flame test using copper which will change to a green-blue flame in
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nutmeg using extraction‚ distillation and recrystallization procedures. This experiment involves extraction and separation techniques that yield a purified product. The product was extracted and a distillation process was used to remove any remaining solvent. The recrystallization of the sample in turn produced a pure sample‚ which was proven using the known melting points of the isolated product. Our outcome led us to a 28 percent recovery of the product. INTRODUCTION Many medications and other
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Alkyl Halides Alkyl halides are a class of compounds where a halogen atom or atoms are bound to an sp3 orbital of an alkyl group. CHCl3 (Chloroform: organic solvent) CF2Cl2 (Freon-12: refrigerant CFC) CF3CHClBr (Halothane: anesthetic) Halogen atoms are more electronegative than carbon atoms‚ and so the C-Hal bond is polarized. H H μ C + C-l δ δ H The C-X bond is polarized in such a way that there is partial positive charge on the carbon and partial negative charge on the halogen. Dipole moment
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