040 grams0.256 grams X 100 % Recovery= 0.16 x 100=16% There are many reasons why the percent recovery is much less than 100%. For example‚ one source of error may have been that the separatory funnel containing the acidified phenylalanine and ethyl acetate may not have separated well enough after being shaken together in the funnel. Not allowing an adequate amount of time for the aqueous and organic layers to separate will cause portions of the layers to be contaminated. This would affect the experimental
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Mapua Institute of Technology Organic Chemistry Laboratory 2 Final Report Factors Affecting the Relative Rates of Electrophilic Aromatic Substitution Reaction Justiniano‚ Priscilla Raiza N. School of Chemical Engineering and Chemistry‚ Mapua Institute of Technology‚ Intramuros‚ Manila‚ Philippines Experiment No.1‚ Submitted on August 6‚ 2011 at N402. Abstract EXPERIMENT NUMBER ONE IS ALL ABOUT THE ELECTROPHILIC SUBSTITUTION OF AROMATIC COMPOUNDS. AROMATIC COMPOUNDS ARE THOSE ORGANIC
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Comparative Investigation of Organic Compounds Tristan Duane G. Lacson‚ Lara Elize T. Lamigo‚ Maria Mikaela L. Laysa‚ Christian Gerard G. Lee and Karen L. Li Group 6 2C Pharmacy Organic Chemistry Laboratory ABSTRACT In order to differentiate the organic compounds. The group tested the compounds using the information based on their instinsic physical properties‚ behavior in ignition‚acidity and basicity and their infrared spectra. The physical properties were noted by the reaserchers by
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Chromatography – Analyzing Analgesics by TLC and Isolation of β-Carotene by Column Chromatography Introduction/Background: Flavonoids are an important group of additives that can be defined as pure substances either natural‚ extracted from raw materials or synthetic. Chromatography is the separation of two or more compounds or ions caused by their molecular interactions with two phases – one moving and one stationary (Weldegirma 2012). Three types of chromatography are used
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separate the mixture of individual compounds from the spinach leaf sample used. Material and apparatus: Part 1 : Analysis of Analgesic Drugs Material: Aspirin Acetaminophen Caffeine Unknown A Unknown B TLC plates Ethyl acetate Hexane Acetic acid Iodine Apparatus: UV Lamp Capillary tube 250mL beaker Filter paper
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Department of Food Science and Technology‚ Faculty of Agriculture‚ AL-Azhar University‚ Cairo‚ Egypt Abstract: This work aimed to evaluate the efficiency of different organic solvents such as‚ methanol‚ ethanol‚ dichloromethane‚ acetone‚ hexane and ethyl acetate for extraction of ( flavonoids and polyphenolic compounds(TFC and TPC respectively) from the orange peel. Also‚ the effect of these solvents on the yield percentage‚ chelating activity‚ antioxidant/radical scavenging capacity and reducing power
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in nonracemic form directly from an achiral precursor. First‚ racemic ibuprofen was converted to aN achiral ketene via the acid chloride by adding thionyl chloride followed by triethylamine. Then‚ ketene was reacted with a chiral and nonracemic (S)-ethyl lactate produces a mixture of diasteromeric esters of ibuprofen derivatives where (S) configuration is predominantly. Finally‚ hydrolysis of the ester then provides (S)-ibuprofen in a relatively high yield. all reaction were monitored by TLC at room
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pigments were separated and concentrated from a crude spinach extract through the use of column chromatography and an eluatropic series of hexanes‚ hexane/acetone‚ and methanol. The pigments were analyzed using thin layer chromatography with a 30% ethyl acetate/hexane developing solvent. Introduction: Chromatography is a technique used to separate a mixture of two or more components based on differences in their physical properties. It can be used as a method of purification (and can be used on
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Introduction Esters are among the most widespread of all naturally occurring compounds. Many simple esters are pleasant-smelling liquids that are responsible for the fragrant odors of fruits and flowers. Examples are benzyl acetate‚ which is finding in orange oil‚ and isopentyl acetate‚ which is the part of banana oil. The ester linkage is also present in animal fats and in many biologically important molecules. Esters can be formed from both organic and inorganic acids and the process of producing
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Although this is a possible reason the desired product still formed. Column chromatography was chosen to purify the compound because it can purify almost any mixture of solids and/or liquids. Using a solvent mixture that was composed of 15% ethyl acetate in hexanes‚ the product eluted straight from the column. It was predicted that the starting material would elute first but there was none present when the column was ran. Since there was not much of a separation‚ what eluted from the column was
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