The masses for the benzoic acid‚ 4- chloroaniline and naphthalene are as follow 2.890 g‚ 3.024 g and 3.036 g. The masses for the three products demonstrates that there was almost an equal amount of product that was extracted for each compound. The beginning mixture was 3.5 g which had equal amounts of the three
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separate Carbose‚ sand‚ and naphthalene? The hypothesis we chose to solve this problem was if we put the mixture into water‚ alcohol‚ and mineral spirts‚ then in each solution one or more substance will not dissolve‚ will be visible‚ and also able to separate. According to our data our hypothesis supported the experiment because CARBOSE and sand are soluble in water while naphthalene is not. The CARBOSE‚ and sand will dissolve in the liquid solvent and the naphthalene will remain in the solid phase
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experiment was to find the eutectic point for the mixture of naphthalene and biphenyl. This was done by measuring the melting point of both pure substances and five mixtures of different ratios. The purpose of the second section was to identify an unknown sample by measuring its melting point and mixing it with two known substances and comparing them. The results suggest that the eutectic point is closest to the weight % ratio of 10/90 naphthalene to biphenyl and the unknown sample is acetamide. Introduction:
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Exercise 1 Binary Solid-Liquid Diagram CHEM 112.1 – 2L Group 2 I. Data and Results Table 1.1 Break and arrest temperature of diphenylamine-naphthalene mixture. Table 1.1. Mole fraction of naphthalene‚ χB‚ and corresponding arrest and break temperature at each run. Run number | Mole Fraction‚XB | Ave. break temperature‚ ˚C | Ave. arrest temperature‚ ˚C | 1 | 1 | 72 | 35.4375 | 2 | 0.868388 | 72 | 35.4375 | 3 | 0.725218 | 62 | 35.4375 | 4 | 0.568895 | 49 | 35.4375
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Retention times (mins): Anthracene 8.67 Benzene 4.37 Naphthalene 5.98 Anthracene standards Peak Area Ratio Sample Concentration Anthracene Benzene A/B 4 2.25 mg/100mL 355003 496920 0.714406746 3 4.5 mg/100mL 583453 467385 1.248334885 2 6.75 mg/100mL 888620 513249 1.73136236 1 9 mg/100mL 1097279 518713 2.115387507 Naphthalene standards Peak Area Ratio Sample Concentration Naphthalene Benzene N/B 4 1.5 mg/100mL 667589 496920 1.343453675
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Experiment B2‚ Heats of Combustion – The Bomb Calorimeter. Objectives: To calibrate a bomb calorimeter by the combustion of benzoic acid. Then to use the calibrated calorimeter to measure the heat of combustion of naphthalene and calculate the heat of formation of naphthalene. Theory: q = C.ΔTBA C = q / ΔTBA Moles = mass / Mr ΔŪ = ΔU / moles ΔHoc‚298 = ΔŪoc‚298 + PDV = ΔŪoc‚298 + RTΔn C10H8 (s) + 12O2 (g) 10CO2 (g) + 4H2O (l) ΔHoc‚298 = - 1
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Colligative Properties 202-NYB-05 (Group 06.) By: Jordan Hribar 1034044 Partner: Anthony Cuillierier Teacher: Daniel Baril Experiment Done: February 23rd‚ 2011 Experiment Number 2. Introduction Some of the properties unique to solutions depend only on the number of dissolved particles and not their identity. Such properties are called colligative properties. The colligative property that will be examined in this experiment will be the freezing point depression as an example
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wavelength Percentage concentration (methanol: water) Peak H value (height equivalent to a theoretical plate) (mm) 230nm 80:20 Phenol 0.0373 Benzophenone 0.0196 Naphthalene 0.0164 235nm 80:20 Phenol 0.0327 Benzophenone 0.0203 Naphthalene 0.0147 260nm 80:20 Phenol 0.0318 Benzophenone 0.0202 Naphthalene 0.0146 Figure 11: table for the height equivalent of the theoretical plates. It can be observed that the H values or height equivalent to a theoretical plate for phenol at the three wavelengths
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a. Draw the Lewis structures of the solute and the solvent. b. Classify the solute and the solvent as polar‚ nonpolar or ionic. c. Identify the solute-solute‚ solvent-solvent and solute-solvent attractive forces. Lewis Structures Solutes: NaCl Naphthalene Glycerol Potassium Iodide Iodine Crystal Solvents: Distilled water Ethyl Alcohol Toluene Solutions Polar‚ Non-Polar or Ionic Attractive Forces NaCl + Distilled Water Solute NaCl Solute-solute Solute-solvent Solvent Distilled
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purity. For ortho-nitrophenol we had 60% recovery and for para 160% recovery. Our melting point ranges were ortho: 45-46°C and para 64-95°C. Introduction: Nitration: In phenols‚ -OH group strongly activates the ring system. As a result‚ phenols are susceptible to oxidation in the presence of concentrated nitric acid (HNO3). Thus‚ nitration of phenols is carried out with dilute nitric acid and results in the formation of o-nitrophenol and p-nitrophenol. The o-nitrophenol is steam volatile and the
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