and Donald Burke Course Instructor Maureen Wilson Lab Title Preparation of cyclohexene from cyclohexanol Aim Preparation of an Alkene by dehydration of an alcohol in the presence of a catalyst. Calculate the percentage recovery of products. Test for purity and identification of products. Abstract Cyclohexene and cyclohexanol are both colourless aromatic compounds. The major difference between the two is the presence of the hydroxyl group present in cyclohexanol. This hydroxyl group can
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Organic Chemistry – Chemistry 226 – Beaulieu Fall 2013 Welcome to Chemistry 226‚ your first semester of organic chemistry! Prepare to be amazed as you develop an entirely new capacity of complex scientific problem solving. This course is a fastpaced‚ action-packed depiction of structure and reactivity of organic molecules. While your chemistry education to date probably has largely overlapped with some biology and physics lectures‚ organic chemistry is like a unique and beautiful snowflake
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Carbon is denoted by the symbol C‚ is part of group 14 on the periodic table‚ and is the fourth most abundant element in the universe (by mass). Carbon has an electron configuration of 1s2‚ 2s2‚ 2p2. With 4 valance shell electrons it is expected to form 4 bonds‚ this means carbon is tetravalent. However the s orbitals do not form the same type of bond (with other atoms) as the p orbitals‚ this is because their shapes are different. For example CH4 would have the following bonds: C(s)-H(s)‚ C(s)-H(s)
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Eqn‚ The Mole‚ Chemical Calculations‚ Acid & Bases 2. Secondary Four Topics- Salts‚ Oxidation & Reduction‚ Metals‚ Electrolysis‚ The Periodic Table‚ Energy Changes‚ Speed of Reaction‚ Ammonia‚ The Atmosphere & environment‚ Organic Chemistry‚ Alkanes‚ Alkenes‚ Alcohols & Carboxylic Acids‚ Macromolecules Physics 1. Secondary Three Topics- Measurement‚ Kinematics‚ Forces‚ Mass Weight & Density‚ Turning Effects of Forces‚ Energy Work & Power‚ Pressure‚ Temperature‚
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recorded. The FTIR was used to confirm that the product was produced. The peaks on the HNMR revealed the presence of aliphatic and aromatic hydrogens and were used to verify the identity of the product. In addition‚ the melting point of the crystals was also used to verify the synthesis of 1‚2-dibromo-1‚2-diphenylethane. Introduction Bromination of an alkene is an example of an addition reaction in which bromine adds across the double bond to form a vicinal dibromide as shown in Figure
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Multistep Synthesis of Tetraphenylcyclopentadienone Author: Instructor: Date work performed: 10.18.2012--10.25.2012 Date work submitted: 11.01.2012 Abstract: The aim of this experiment was to perform a multistep synthesis to form tetraphenylcyclopentadienone. The first step of the reactions was to synthesize benzoin from the condensation of benzaldehyde. A yield of 28.91% benzoin was obtained. The MP of benzoin was 127O-130O C and the IR spectra displayed a carbonyl peak at 3415 cm-1
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HSC Chemistry Topic 1 PRODUCT ON of MATERIALS What is this topic about? To keep it as simple as possible‚ (K.I.S.S.) this topic involves the study of: 1. POLYMERS FROM PETROCHEMICALS & BIOMASS 2. ALTERNATIVE FUELS - ETHANOL & THE ALKANOLS 3. REDOX CHEMISTRY & BATTERIES 4. RADIOACTIVITY & ITS USES ...all in the context of society’s use of energy and materials but first) an introduction ... In the previous topic in the Preliminary Course‚ you learnt about carbon chemistry of petroleum Then you
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Steam distillation of cloves produced 0.53g of an oil which contained in its IR spectrum the functional groups O-H (at 3520 cm-1)‚ sp2 C-H (3080 – 3000 cm-1)‚ aliphatic C-H (2980 – 2940 cm-1)‚ and both alkene C=C (at 1640 cm-1) and aromatic C=C (at 1514 cm-1). The IR spectrum is attached to this report. These data are consistent with the structure of eugenol‚ shown in Figure 2 below: In addition‚ the IR of the product from the steam distillation of cloves closely corresponds with that of an
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Identification of Unknown Organic Compounds by Melting Point‚ Boiling Point‚ and Infrared Spectroscopy Methods and Background The goal of this laboratory experiment was to determine the structure and identity of an unknown solid and an unknown liquid by using elemental analysis‚ index of hydrogen deficiency‚ infrared spectroscopy‚ melting point (for solid)‚ and boiling point (for liquid). In this laboratory‚ we were given unknown solid “C” and unknown liquid “D”. The empirical formula
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Gaseous State Start Practice | Polymers Start Practice | | | "Do if you have Time" Chapters | Aldehyde Ketone Start Practice | Solutions Start Practice | Solid State Start Practice | Mole Concepts Start Practice | Alkanes‚ Alkenes and Alk... Start Practice | Surface Chemistry Start Practice | Nuclear Chemistry Start Practice | Purification Characteriz... Start Practice | Environmental Chemistry Start Practice | Electrochemistry Start Practice | |
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