oil with an aromatic spicy odor. Acetyleugenol 0.528 5.28 Clear to pale yellow oily liquid with aromatic spicy odor. Calculations Percent recovery of eugenol Amt. Eugenol isolated 0.712 g % Recovery = ------------------------------ = -------------- x 100 = 7.12 % Amt. Cloves used 10 g IR spectrograph: See IR graph attached Conclusion Simple distillation of whole cloves produced 0.712 g of a yellow oil with spicy aromatic odor‚ which
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other halogens and interhalogens‚ RCOOH‚ HsiR3‚ alkyl‚ aryl‚ vinyl‚ and benzylhalides‚ acyls RC(O)Cl and O2. Substrates with A [pic]B usually add to the metal with retention of an A[pic]B single bond. For example‚ aldehydes‚ ketones‚ alkenes and alkynes‚ particularay with electron withdrawing substituents‚ can undergo reactions which amount to an oxidative addition to the metal: [pic] Of course the readiness of the metal center to react with potentially oxidative substrates depends
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Multistep Synthesis of Tetraphenylcyclopentadienone In this laboratory experiment a synthesis was performed through several separate steps. The purpose of the experiment was to synthesize tetraphenylcyclopentadienone from benzaldehyde and to run reactions on carbonyl containing compounds. There was a total of three steps that led up to the synthesis of the final product‚ tetraphenylcyclopentadienone. The first step of the experiment was the condensation of benzaldehyde to yield
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Esmeralda Curiel Organic Chemistry October 21‚ 2014 Experiment 41- 1‚4-Diphenyl-1‚3-Butadiene INTRODUCTION The study of the Wittig Reaction is important because it is often used to form alkenes from carbonyl compounds. The purpose of this experiment is to isolate the trans‚ trans-1‚4-diphenyl-1‚3-butadiene‚ which is formed by a Wittig reaction along with the cis‚ trans isomeric diene. The reaction is carried out in two steps. First the Wittig salt is obtained through a simple nucleophilic displacement
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ALCOHOLS Alcohols are compounds in which one or more hydrogen atoms in an alkane have been replaced by an -OH group. For the purposes of UK A level‚ we will only look at compounds containing one -OH group. For example: Primary alcohols In a primary (1°) alcohol‚ the carbon which carries the -OH group is only attached to one alkyl group Some examples of primary alcohols include: Secondary alcohols In a secondary (2°) alcohol‚ the carbon with the -OH group attached is joined directly to
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Contents PART XV ANALYTICAL CHEMISTRY Chapter 63 Detecting the presence of chemical species Action of heating solid sample strongly 1 Chapter 64 Separation and purification methods Centrifugation Sublimation Partition equilibrium of a solute between two immiscible solvents Two-dimensional thin-layer chromatography 2 2 3 6 Chapter 65 Quantitative methods of analysis Detection of end point in acid-alkali titration 8 Chapter 66 Instrumental analytical methods More
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(note: there is CO2 solid‚ its dry ice) – Complete combustion: ▪ hydrocarbon + oxygen [pic] water + carbon dioxide – Displacement reactions: ▪ Y + X (anion)[pic] X + Y (anion); where Y > X on activity series or Eo table. • Alkene/alkane reactions: – Cracking of pentane: ▪ pentane [pic] ethylene + propane ▪ C5H12 (g) [pic] C2H4 (g) + C3H8 (g) – Hydration of ethylene (the reverse can also happen known as de-hydration‚ where concentrated acid is used):
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Chemistry Essay Butane‚ Butene and all isomers that come with them are considered to be alkanes and alkenes respectively. They differ from each other in the fact that Butane contains only single bonds‚ whereas Butene has both single and one double bond. Regardless of this difference in many situations the two molecules can display similar behaviours. For the purposes of this comparison But-1-ene will be used as ‘Butene’ unless otherwise indicated. But-1-ene is almost identical to the other
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One major observation made throughout this experiment was during the steam distillation. As the steam distillation started and the solution in the flask began heating‚ it was clear that too much stopcock grease was used around the glassware. The grease from the connecting ends of the three way connecting tube was melting and seeping into the clove and water solution in the two necked round bottom flask. The solution in the flask was immediately discarded and repeated with clean glassware and a very
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showed a CP spot‚ indicating that the reaction had gone to completion. 3. IR Spectroscopy Peaks Peak Functional Group1 2362.05 cm-1 Very weak band 1712.90 cm-1 (Strongest peak) C=O (ketone) 1598.22 cm-1 C=C (aromatic) 1450.50 cm-1 C=C (aromatic) 1150.63 cm-1 Very weak band 735.43 cm-1 =C–H (alkene) 669.78 cm-1 Very weak band Attached is a published spectrum from: http://sdbs.db.aist.go.jp/sdbs/cgi-bin/direct_frame_top.cgi Discussion 1. According to the melting point measured‚ the final product was
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